Technology Process of C34H50F3N7O10SSi2
There total 5 articles about C34H50F3N7O10SSi2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dmap; triethylamine;
In
dichloromethane;
at 0 ℃;
for 0.25h;
DOI:10.1021/cb200510k
- Guidance literature:
-
Multi-step reaction with 5 steps
1: N,N-dimethyl-formamide / 6 h / 20 °C
2: di-isopropyl azodicarboxylate; triphenylphosphine / 1,4-dioxane / 16 h / 20 °C
3: dmap / dichloromethane / 0.5 h / 0 °C
4: 18-crown-6 ether; potassium trifluoroacetate; N-ethyl-N,N-diisopropylamine / toluene / 16 h / 80 °C
5: dmap; triethylamine / dichloromethane / 0.25 h / 0 °C
With
dmap; 18-crown-6 ether; di-isopropyl azodicarboxylate; potassium trifluoroacetate; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine;
In
1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/cb200510k
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 18-crown-6 ether; potassium trifluoroacetate; N-ethyl-N,N-diisopropylamine / toluene / 16 h / 80 °C
2: dmap; triethylamine / dichloromethane / 0.25 h / 0 °C
With
dmap; 18-crown-6 ether; potassium trifluoroacetate; triethylamine; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; toluene;
DOI:10.1021/cb200510k
