[4,5-bis(2,4,6-trimethylphenoxy)-9-anthryl]dimethoxyborane

Base Information

Chemical Name:[4,5-bis(2,4,6-trimethylphenoxy)-9-anthryl]dimethoxyborane
CAS No.:1376607-94-1
Molecular Formula:C₃₄H₃₅BO₄
Molecular Weight:518.46
Hs Code.:

Synonyms:[4,5-bis(2,4,6-trimethylphenoxy)-9-anthryl]dimethoxyborane

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Chemical Property of [4,5-bis(2,4,6-trimethylphenoxy)-9-anthryl]dimethoxyborane

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Technology Process of [4,5-bis(2,4,6-trimethylphenoxy)-9-anthryl]dimethoxyborane

There total 1 articles about [4,5-bis(2,4,6-trimethylphenoxy)-9-anthryl]dimethoxyborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 121-43-7,63156-11-6
Trimethyl borate

: 1260156-77-1
4,5-bis(2,4,6-trimethylphenoxy)-9-bromoanthracene

: 1376607-94-1
[4,5-bis(2,4,6-trimethylphenoxy)-9-anthryl]dimethoxyborane

Guidance literature:: 4,5-bis(2,4,6-trimethylphenoxy)-9-bromoanthracene; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

Trimethyl borate; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1021/ja3036042

Reference yield: 27.0%

: 1376607-97-4
4-bromo-3-iodobenzo[b]thiophene

: 1376607-94-1
[4,5-bis(2,4,6-trimethylphenoxy)-9-anthryl]dimethoxyborane

: 1376608-00-2
[4,5-bis(2,4,6-trimethylphenoxy)-9-anthryl]-bis(4-bromobenzo[b]thiophen-3-yl)borane

Guidance literature:: With n-C₄H₉Li; In diethyl ether; C8H4SBrI reacted with n-C4H9Li in Et2O at -78°C, reacted with B compd.; chromd. (silica gel);
DOI:10.1021/ja3036042

Reference yield:

: 1376607-94-1
[4,5-bis(2,4,6-trimethylphenoxy)-9-anthryl]dimethoxyborane

: 1376607-93-0
C₃₀H₁₁BS₂(OC₆H₂(CH₃)3)2

Guidance literature:: Multi-step reaction with 3 steps

1: n-C₄H₉Li / diethyl ether

2: ((CH₃)3Si)3SiH; 1,1'-azobis(cyclohexanecarbonitrile) / toluene

3: FeCl₃ / dichloromethane; nitromethane

With n-C₄H₉Li; ((CH₃)3Si)3SiH; 1,1'-azobis(cyclohexanecarbonitrile); FeCl₃; In diethyl ether; nitromethane; dichloromethane; toluene;
DOI:10.1021/ja3036042