γ-(benzyloxycarbonylamino)butanoic acid 2,2,2-trichloroethyl ester

Base Information

Chemical Name:γ-(benzyloxycarbonylamino)butanoic acid 2,2,2-trichloroethyl ester
CAS No.:544445-13-8
Molecular Formula:C₁₄H₁₆Cl₃NO₄
Molecular Weight:368.644
Hs Code.:

Synonyms:γ-(benzyloxycarbonylamino)butanoic acid 2,2,2-trichloroethyl ester

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Chemical Property of γ-(benzyloxycarbonylamino)butanoic acid 2,2,2-trichloroethyl ester

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Technology Process of γ-(benzyloxycarbonylamino)butanoic acid 2,2,2-trichloroethyl ester

There total 1 articles about γ-(benzyloxycarbonylamino)butanoic acid 2,2,2-trichloroethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 115-20-8
1,1,1-trichloroethanol

: 5105-78-2
4-(benzyloxycarbonylamino)butyric acid

: 544445-13-8
γ-(benzyloxycarbonylamino)butanoic acid 2,2,2-trichloroethyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jo061871f

Reference yield: 82.0%

: 4304-12-5
(2R,3R,4S,5S,6R)-2-(benzyloxy)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4,5-triol

: 544445-13-8
γ-(benzyloxycarbonylamino)butanoic acid 2,2,2-trichloroethyl ester

: 4-Benzyloxycarbonylamino-butyric acid (2R,3S,4S,5R,6R)-6-benzyloxy-3,4,5-trihydroxy-tetrahydro-pyran-2-ylmethyl ester

Guidance literature:: With 4 A molecular sieve; Novozym 435 (immobilized Candida antartica lipase); In acetonitrile; at 45 ℃; for 29h;
DOI:10.1016/S0040-4039(03)00223-5

Reference yield:

: 544445-13-8
γ-(benzyloxycarbonylamino)butanoic acid 2,2,2-trichloroethyl ester

: 115-20-8
1,1,1-trichloroethanol

: 5105-78-2
4-(benzyloxycarbonylamino)butyric acid

Guidance literature:: With phosphate buffer; Bacillus subtilis esterase BS₂; In methanol; hexane; at 37 ℃; for 0.25h; pH=7.4; Further Variations:; reaction times; enzyme/substrate ratios; Product distribution;
DOI:10.1021/jo061871f