O-[alpha-(2-benzothiazolyl)-2,4-dichlorobenzyl]-O-ethyl-S-n-propyl thiophosphate

Base Information

Chemical Name:O-[alpha-(2-benzothiazolyl)-2,4-dichlorobenzyl]-O-ethyl-S-n-propyl thiophosphate
CAS No.:89204-65-9
Molecular Formula:C₁₉H₂₀Cl₂NO₃PS₂
Molecular Weight:476.384
Hs Code.:

Synonyms:O-[alpha-(2-benzothiazolyl)-2,4-dichlorobenzyl]-O-ethyl-S-n-propyl thiophosphate

Suppliers and Price of O-[alpha-(2-benzothiazolyl)-2,4-dichlorobenzyl]-O-ethyl-S-n-propyl thiophosphate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of O-[alpha-(2-benzothiazolyl)-2,4-dichlorobenzyl]-O-ethyl-S-n-propyl thiophosphate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of O-[alpha-(2-benzothiazolyl)-2,4-dichlorobenzyl]-O-ethyl-S-n-propyl thiophosphate

There total 4 articles about O-[alpha-(2-benzothiazolyl)-2,4-dichlorobenzyl]-O-ethyl-S-n-propyl thiophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.0%

: 7651-98-1
O-ethyl-S-propyl phosphorochloridate

: 96327-87-6
Benzothiazol-2-yl-(2,4-dichloro-phenyl)-methanol

: 89204-65-9
O-[alpha-(2-benzothiazolyl)-2,4-dichlorobenzyl]-O-ethyl-S-n-propyl thiophosphate

Guidance literature:: With triethylamine; In dichloromethane; at 25 ℃;
DOI:10.1021/jo00212a017

Reference yield:

: 95-16-9
1,3-Benzothiazole

: 89204-65-9
O-[alpha-(2-benzothiazolyl)-2,4-dichlorobenzyl]-O-ethyl-S-n-propyl thiophosphate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-butyllithium / 1.) Et₂O, -78 deg C, 0.5 h, 2.) 25 deg C, overnight

2: 9 percent / triethylamine / CH₂Cl₂ / 25 °C

With n-butyllithium; triethylamine; In dichloromethane;
DOI:10.1021/jo00212a017

Reference yield:

: 874-42-0
2,4-dichlorobenzaldeyhde

: 89204-65-9
O-[alpha-(2-benzothiazolyl)-2,4-dichlorobenzyl]-O-ethyl-S-n-propyl thiophosphate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-butyllithium / 1.) Et₂O, -78 deg C, 0.5 h, 2.) 25 deg C, overnight

2: 9 percent / triethylamine / CH₂Cl₂ / 25 °C

With n-butyllithium; triethylamine; In dichloromethane;
DOI:10.1021/jo00212a017