di(p-tolyl)(3-pyridyl)amine

Base Information

Chemical Name:di(p-tolyl)(3-pyridyl)amine
CAS No.:325989-55-7
Molecular Formula:C₁₉H₁₈N₂
Molecular Weight:274.365
Hs Code.:

Synonyms:di(p-tolyl)(3-pyridyl)amine

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Chemical Property of di(p-tolyl)(3-pyridyl)amine

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Technology Process of di(p-tolyl)(3-pyridyl)amine

There total 1 articles about di(p-tolyl)(3-pyridyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1120-90-7
3-iodopyridine

: 620-93-9
di-p-tolylamine

: 325989-55-7
di(p-tolyl)(3-pyridyl)amine

Guidance literature:: With copper(l) iodide; 1,10-Phenanthroline; potassium tert-butylate; In toluene; at 110 - 115 ℃; for 12h;
DOI:10.1021/ic200966f

Reference yield: 80.0%

: ammonium hexafluorophosphate

: 345911-20-8,19542-80-4,158060-65-2,34795-02-3,15746-57-3
cis-dichlorobis(2,2′-bipyridine)ruthenium(II)

: 325989-55-7
di(p-tolyl)(3-pyridyl)amine

: 7732-18-5
water

: Ru((C₅H₄N)2)2(NC₅H₄N(C₆H₄CH₃)2)2⁽²⁺⁾*2PF₆^(1-)=Ru((C₅H₄N)2)2(NC₅H₄N(C₆H₄CH₃)2)2(PF₆)2

Guidance literature:: In water; (Ar); heating a suspn. of Ru complex in water to 90°C for 1 h, addn. of a soln. of ligand in ethanol, heating with stirring at 90°C for 12 h in darkness, filtration, addn. of satd. NH4PF6; filtration, washing with colf water in the dark;
DOI:10.1021/ic200966f

Reference yield: 70.0%

: ammonium hexafluorophosphate

: 345911-20-8,19542-80-4,158060-65-2,34795-02-3,15746-57-3
cis-dichlorobis(2,2′-bipyridine)ruthenium(II)

: 325989-55-7
di(p-tolyl)(3-pyridyl)amine

: 1354627-30-7
Ru((C₅H₄N)2)2Cl(NC₅H₄N(C₆H₄CH₃)2)⁽¹⁺⁾*PF₆^(1-)=Ru((C₅H₄N)2)2Cl(NC₅H₄N(C₆H₄CH₃)2)PF₆

Guidance literature:: With LiCl; In ethanol; water; (Ar); addn. of ligand and LiCl to a suspn. of Ru complex in ethanol/water in the dark, heating to 90°C, evapn. in darkness, dissolving inwater, addn. of aq. NH4PF6; filtration, washing with colf water in the dark;
DOI:10.1021/ic200966f