6-<5-β-(N-methyl-N-trifluoroacetylamino)ethyl-2-methoxy>phenyloxyveratric acid

Base Information

Chemical Name:6-<5-β-(N-methyl-N-trifluoroacetylamino)ethyl-2-methoxy>phenyloxyveratric acid
CAS No.:142609-34-5
Molecular Formula:C₂₁H₂₂F₃NO₇
Molecular Weight:457.403
Hs Code.:

Synonyms:6-<5-β-(N-methyl-N-trifluoroacetylamino)ethyl-2-methoxy>phenyloxyveratric acid

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Chemical Property of 6-<5-β-(N-methyl-N-trifluoroacetylamino)ethyl-2-methoxy>phenyloxyveratric acid

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Technology Process of 6-<5-β-(N-methyl-N-trifluoroacetylamino)ethyl-2-methoxy>phenyloxyveratric acid

There total 6 articles about 6-<5-β-(N-methyl-N-trifluoroacetylamino)ethyl-2-methoxy>phenyloxyveratric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 142609-33-4
6-<5-β-(N-methyl-N-trifluoroacetylamino)ethyl-2-methoxy>phenyloxyveratraldehyde

: 142609-34-5
6-<5-β-(N-methyl-N-trifluoroacetylamino)ethyl-2-methoxy>phenyloxyveratric acid

Guidance literature:: With potassium permanganate; magnesium sulfate; In acetone; for 3h; Heating;

Reference yield:

: 68360-20-3
N-formyl-3-benzyloxy-4-methoxyphenethylamine

: 142609-34-5
6-<5-β-(N-methyl-N-trifluoroacetylamino)ethyl-2-methoxy>phenyloxyveratric acid

Guidance literature:: Multi-step reaction with 5 steps

1: 382 mg / LiAlH₄ / tetrahydrofuran; diethyl ether / 1.) 20 min, RT, 2.) 50 deg C, 6 h

2: K₂CO₃ / CH₂Cl₂ / 1 h / Ambient temperature

3: 85 percent / H₂ / 2percent PdCl₂, C / methanol / 760 Torr

4: 49 percent / K₂CO₃, CuO, pyridine / 13 h / Heating

5: 68 percent / 1percent aq. KMnO₄, MgSO₄ / acetone / 3 h / Heating

With pyridine; potassium permanganate; lithium aluminium tetrahydride; hydrogen; magnesium sulfate; potassium carbonate; copper(II) oxide; palladium dichloride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; acetone;

Reference yield:

: 36455-21-7
3-benzyloxy-4-methoxyphenylethylamine

: 142609-34-5
6-<5-β-(N-methyl-N-trifluoroacetylamino)ethyl-2-methoxy>phenyloxyveratric acid

Guidance literature:: Multi-step reaction with 6 steps

1: 89 percent / 6 h / Heating

2: 382 mg / LiAlH₄ / tetrahydrofuran; diethyl ether / 1.) 20 min, RT, 2.) 50 deg C, 6 h

3: K₂CO₃ / CH₂Cl₂ / 1 h / Ambient temperature

4: 85 percent / H₂ / 2percent PdCl₂, C / methanol / 760 Torr

5: 49 percent / K₂CO₃, CuO, pyridine / 13 h / Heating

6: 68 percent / 1percent aq. KMnO₄, MgSO₄ / acetone / 3 h / Heating

With pyridine; potassium permanganate; lithium aluminium tetrahydride; hydrogen; magnesium sulfate; potassium carbonate; copper(II) oxide; palladium dichloride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; acetone;