<2-allylglycine>-RA-VII

Base Information

Chemical Name:<2-allylglycine>-RA-VII
CAS No.:153445-52-4
Molecular Formula:C₄₃H₅₂N₆O₉
Molecular Weight:796.921
Hs Code.:

Synonyms:<2-allylglycine>-RA-VII

Suppliers and Price of <2-allylglycine>-RA-VII

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of <2-allylglycine>-RA-VII

Chemical Property:

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Technology Process of <2-allylglycine>-RA-VII

There total 3 articles about <2-allylglycine>-RA-VII which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 140679-95-4
RA-X methyl ester

: 153445-52-4
<2-allylglycine>-RA-VII

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / LiBH₄ / tetrahydrofuran / 12 h / Ambient temperature

2: 96 percent / DMAP, Et₃N / CH₂Cl₂ / 1 h / -78 °C

3: 1.) o-nitrophenylselenecyanate, NaBH₄, 2.) 35percent aq. H₂O₂ / 1.) EtOH, RT, 3 h, 2.) THF-EtOH, RT, 12 h

With dmap; sodium tetrahydroborate; lithium borohydride; ortho-nitrophenyl selenocyanate; dihydrogen peroxide; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1248/cpb.41.1402

Reference yield:

: 153445-49-9
<2-(δ-hydroxynorvaline)>-RA-VII

: 153445-52-4
<2-allylglycine>-RA-VII

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / DMAP, Et₃N / CH₂Cl₂ / 1 h / -78 °C

2: 1.) o-nitrophenylselenecyanate, NaBH₄, 2.) 35percent aq. H₂O₂ / 1.) EtOH, RT, 3 h, 2.) THF-EtOH, RT, 12 h

With dmap; sodium tetrahydroborate; ortho-nitrophenyl selenocyanate; dihydrogen peroxide; triethylamine; In dichloromethane;
DOI:10.1248/cpb.41.1402

Reference yield:

: 153445-50-2
<2-(δ-hydroxynorvaline)>-RA-VII mesylate

: 153445-52-4
<2-allylglycine>-RA-VII

Guidance literature:: With sodium tetrahydroborate; ortho-nitrophenyl selenocyanate; dihydrogen peroxide; Yield given. Multistep reaction; 1.) EtOH, RT, 3 h, 2.) THF-EtOH, RT, 12 h;
DOI:10.1248/cpb.41.1402