7-(4-chlorophenyl)-5-methylbenzo[d]thiazol-6-yl trifluoromethanesulfonate

Base Information

Chemical Name:7-(4-chlorophenyl)-5-methylbenzo[d]thiazol-6-yl trifluoromethanesulfonate
CAS No.:1403665-95-1
Molecular Formula:C₁₅H₉ClF₃NO₃S₂
Molecular Weight:407.822
Hs Code.:

Synonyms:7-(4-chlorophenyl)-5-methylbenzo[d]thiazol-6-yl trifluoromethanesulfonate

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Chemical Property of 7-(4-chlorophenyl)-5-methylbenzo[d]thiazol-6-yl trifluoromethanesulfonate

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Technology Process of 7-(4-chlorophenyl)-5-methylbenzo[d]thiazol-6-yl trifluoromethanesulfonate

There total 5 articles about 7-(4-chlorophenyl)-5-methylbenzo[d]thiazol-6-yl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 136-90-3
4-methoxy-3-methylaniline

: 1403665-95-1
7-(4-chlorophenyl)-5-methylbenzo[d]thiazol-6-yl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 6 steps

1.1: acetic acid / 0.75 h / 0 - 20 °C

1.2: 0 - 20 °C

2.1: sodium nitrite; phosphoric acid / water / 0.33 h / 0 °C

2.2: 20 °C / Cooling with ice

3.1: boron tribromide / dichloromethane / 2 h / 0 °C

4.1: bromine; acetic acid / 1 h / 20 °C

5.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 0.17 h / 110 °C / Microwave irradiation

6.1: pyridine / dichloromethane / 1 h / 0 °C

With pyridine; phosphoric acid; bromine; boron tribromide; potassium carbonate; acetic acid; sodium nitrite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; dichloromethane; water;

Reference yield:

: 1403665-93-9
7-bromo-5-methylbenzo[d]thiazol-6-ol

: 1403665-95-1
7-(4-chlorophenyl)-5-methylbenzo[d]thiazol-6-yl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 0.17 h / 110 °C / Microwave irradiation

2: pyridine / dichloromethane / 1 h / 0 °C

With pyridine; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; dichloromethane; water;

Reference yield:

: 1403665-90-6
2-amino-6-methoxy-5-methylbenzothiazole

: 1403665-95-1
7-(4-chlorophenyl)-5-methylbenzo[d]thiazol-6-yl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium nitrite; phosphoric acid / water / 0.33 h / 0 °C

1.2: 20 °C / Cooling with ice

2.1: boron tribromide / dichloromethane / 2 h / 0 °C

3.1: bromine; acetic acid / 1 h / 20 °C

4.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 0.17 h / 110 °C / Microwave irradiation

5.1: pyridine / dichloromethane / 1 h / 0 °C

With pyridine; phosphoric acid; bromine; boron tribromide; potassium carbonate; acetic acid; sodium nitrite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; dichloromethane; water;