C₂₉H₄₈INO₃Si

Base Information Edit

Chemical Name:C₂₉H₄₈INO₃Si
CAS No.:1072091-21-4
Molecular Formula:C₂₉H₄₈INO₃Si
Molecular Weight:613.695
Hs Code.:
Mol file:1072091-21-4.mol

C<sub>29</sub>H<sub>48</sub>INO<sub>3</sub>Si

Synonyms:C₂₉H₄₈INO₃Si

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Chemical Property of C₂₉H₄₈INO₃Si Edit

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Technology Process of C₂₉H₄₈INO₃Si

There total 8 articles about C₂₉H₄₈INO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1072091-19-0
C₂HF₃O₂*C₁₆H₂₂INO

: 1072091-21-4
C₂₉H₄₈INO₃Si

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 1.5h;

Reference yield:

: 1072091-12-3
(2R,3S,4E)-6-(benzyloxy)-3-[(4-methoxyphenyl)amino]-2,4-dimethylhex-4-en-1-ol

: 1072091-21-4
C₂₉H₄₈INO₃Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuric acid; periodic acid / water; acetonitrile / 1.5 h / 20 °C

1.2: 8 h / 20 °C

2.1: Dess-Martin periodane / dichloromethane / 0.17 h / 20 °C

3.1: chromium dichloride / tetrahydrofuran / 5.5 h / 0 - 20 °C

4.1: dichloromethane / 3 h / 20 °C

5.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 1.5 h / 20 °C

With chromium dichloride; sulfuric acid; benzotriazol-1-ol; Dess-Martin periodane; periodic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1072091-14-5
tert-butyl {(1S,2E)-4-(benzyloxy)-1-[(1R)-2-hydroxy-1-methylethyl]-2-methylbut-2-en-1-yl}carbamate

: 1072091-21-4
C₂₉H₄₈INO₃Si

Guidance literature:: Multi-step reaction with 4 steps

1: Dess-Martin periodane / dichloromethane / 0.17 h / 20 °C

2: chromium dichloride / tetrahydrofuran / 5.5 h / 0 - 20 °C

3: dichloromethane / 3 h / 20 °C

4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 1.5 h / 20 °C

With chromium dichloride; benzotriazol-1-ol; Dess-Martin periodane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;