N-[(1R)-1-Methylpropyl]benzamide

Base Information

Chemical Name:N-[(1R)-1-Methylpropyl]benzamide
CAS No.:13250-13-0
Molecular Formula:C₁₁H₁₅NO
Molecular Weight:177.246
Hs Code.:
DSSTox Substance ID:DTXSID301301220
Nikkaji Number:J52.836F

Synonyms:SCHEMBL8507346;DTXSID301301220;(?)-N-[(R)-sec-Butyl]benzamide;N-[(1R)-1-Methylpropyl]benzamide;13250-13-0

Suppliers and Price of N-[(1R)-1-Methylpropyl]benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of N-[(1R)-1-Methylpropyl]benzamide

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:177.115364102
Heavy Atom Count:13
Complexity:162

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCC(C)NC(=O)C1=CC=CC=C1
Isomeric SMILES:CC[C@@H](C)NC(=O)C1=CC=CC=C1

Technology Process of N-[(1R)-1-Methylpropyl]benzamide

There total 10 articles about N-[(1R)-1-Methylpropyl]benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 13250-12-9
(R)-sec-butylamine

: 100-51-6,185532-71-2
benzyl alcohol

: 13250-13-0
(R)-N-(1-methylpropyl)benzamide

Guidance literature:: With potassium tert-butylate; [Ru(P^tBuNNH^Bn)H(CO)Cl]; In tert-butyl methyl ether; at 70 ℃; for 60h; under 760.051 Torr; Inert atmosphere;
DOI:10.1021/acscatal.1c00728

Reference yield:

: 952524-02-6
(S)-1-benzoyl-2-(α-acetoxyethyl)benzimidazole

: 33966-50-6
SEC-BUTYLAMINE

: 513-49-5
(S)-2-aminobutane

: 13250-12-9
(R)-sec-butylamine

: 22526-49-4
(S)-N-(1-methylpropyl)benzamide

: 13250-13-0
(R)-N-(1-methylpropyl)benzamide

Guidance literature:: In tetrahydrofuran; at -10 ℃; for 12h; Title compound not separated from byproducts.;
DOI:10.1016/j.tetasy.2007.12.006

Reference yield:

: 106-98-9,9003-28-5
1-butylene

: 98-88-4
benzoyl chloride

: 22526-49-4
(S)-N-(1-methylpropyl)benzamide

: 13250-13-0
(R)-N-(1-methylpropyl)benzamide

Guidance literature:: 1-butylene; With phenylsilane; C₂₉H₃₀N₄; cobalt(II) acetate; tert-butyl 2-diazo-2-phenylacetate; In 2-ethoxy-ethanol; ethyl acetate; at -10 ℃; for 24h; Schlenk technique; Inert atmosphere;

With acetic acid; zinc; In tetrahydrofuran; water; at 50 ℃; for 3h;

benzoyl chloride; With triethylamine; In tetrahydrofuran; diethyl ether; at 20 ℃; for 3h; Overall yield = 67 percent;