phenyl 3,4,6-tri-O-benzyl-2-O-(diphenoxy phosphonoyl)-β-D-thioglucopyranoside

Base Information

Chemical Name:phenyl 3,4,6-tri-O-benzyl-2-O-(diphenoxy phosphonoyl)-β-D-thioglucopyranoside
CAS No.:906359-92-0
Molecular Formula:C₄₅H₄₃O₈PS
Molecular Weight:774.871
Hs Code.:

Synonyms:phenyl 3,4,6-tri-O-benzyl-2-O-(diphenoxy phosphonoyl)-β-D-thioglucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl 3,4,6-tri-O-benzyl-2-O-(diphenoxy phosphonoyl)-β-D-thioglucopyranoside

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Technology Process of phenyl 3,4,6-tri-O-benzyl-2-O-(diphenoxy phosphonoyl)-β-D-thioglucopyranoside

There total 2 articles about phenyl 3,4,6-tri-O-benzyl-2-O-(diphenoxy phosphonoyl)-β-D-thioglucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 127299-77-8,130781-28-1,138181-68-7,130781-27-0
Phenyl 3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 906359-92-0
phenyl 3,4,6-tri-O-benzyl-2-O-(diphenoxy phosphonoyl)-β-D-thioglucopyranoside

Guidance literature:: With sodium hydride; In various solvent(s);
DOI:10.1002/anie.200602699

Reference yield: 57.0%

: 906359-92-0
phenyl 3,4,6-tri-O-benzyl-2-O-(diphenoxy phosphonoyl)-β-D-thioglucopyranoside

Guidance literature:

Reference yield: 84.0%

: 906359-92-0
phenyl 3,4,6-tri-O-benzyl-2-O-(diphenoxy phosphonoyl)-β-D-thioglucopyranoside

: 108-93-0
cyclohexanol

: C₄₅H₄₉O₉P

Guidance literature:: phenyl 3,4,6-tri-O-benzyl-2-O-(diphenoxy phosphonoyl)-β-D-thioglucopyranoside; With 2,6-di-tert-butyl-4-methylpyridine; 1-(phenylsulphenyl)piperidylamide; trifluoromethylsulfonic anhydride; In dichloromethane; at -60 ℃;

cyclohexanol; In dichloromethane; at -60 ℃; Further stages.;
DOI:10.1002/anie.200602699