3-Benzofuranmethanamine, N-methyl-

Base Information

• Chemical Name: 3-Benzofuranmethanamine, N-methyl-
• CAS No.: 78629-16-0
• Molecular Formula: C10H11 N O
• Molecular Weight: 161.203
• Hs Code.: 2932999099
• Mol file: 78629-16-0.mol

Synonyms:3-Benzofuranmethanamine, N-methyl-

Chemical Property of 3-Benzofuranmethanamine, N-methyl-

Chemical Property:

• PSA: 25.17000
• LogP: 2.54310

Purity/Quality:

(1-Benzofuran-3-ylmethyl)methylamine hydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Benzofuranmethanamine, N-methyl-

There total 1 articles about 3-Benzofuranmethanamine, N-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1-benzofuran-3-carbaldehyde (4687-25-6) + methylamine (74-89-5) → N-methyl-3-benzofuranmethanamine (78629-16-0)

Guidance literature:

1-benzofuran-3-carbaldehyde; methylamine; In methanol; at 20 ℃; for 4h;

With sodium tetrahydroborate; In methanol; at 0 ℃; for 0.166667h;

Reference yield: 67.0%

Cinnamyl bromide (4392-24-9) + N-methyl-3-benzofuranmethanamine (78629-16-0) → (E)-N-methyl-N-(3-phenyl-2-propenyl)-3-benzofuranmethanamine (98977-77-6)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield: 61.0%

(E)-4-(3-bromoprop-1-en-1-yl)-1,1'-biphenyl (113538-24-2) + N-methyl-3-benzofuranmethanamine (78629-16-0) → (E)-3-([1,1'-biphenyl]-4-yl)-N-(benzofuran-3-ylmethyl)-N-methylprop-2-en-1-amine hydrochloride

Guidance literature:

(E)-4-(3-bromoprop-1-en-1-yl)-1,1'-biphenyl; N-methyl-3-benzofuranmethanamine; With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;

With hydrogenchloride; at 20 ℃; for 0.266667h;

DOI:10.1021/acs.jmedchem.7b01300

upstream raw materials:

1-benzofuran-3-carbaldehyde

methylamine

Downstream raw materials:

(E)-N-methyl-N-(3-phenyl-2-propenyl)-3-benzofuranmethanamine

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