3,5-Cyclohexadiene-1,2-dione,3-methyl-6-(1-methylethyl)-(9CI)

Base Information

• Chemical Name: 3,5-Cyclohexadiene-1,2-dione,3-methyl-6-(1-methylethyl)-(9CI)
• CAS No.: 78617-27-3
• Molecular Formula: C10H12 O2
• Molecular Weight: 164.204
• Mol file: 78617-27-3.mol

Synonyms:3,5-Cyclohexadiene-1,2-dione,3-methyl-6-(1-methylethyl)-(9CI)

Chemical Property of 3,5-Cyclohexadiene-1,2-dione,3-methyl-6-(1-methylethyl)-(9CI)

Chemical Property:

• PSA: 34.14000
• LogP: 1.66690

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,5-Cyclohexadiene-1,2-dione,3-methyl-6-(1-methylethyl)-(9CI)

There total 7 articles about 3,5-Cyclohexadiene-1,2-dione,3-methyl-6-(1-methylethyl)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

3-isopropyl-6-methyl-1,2-benzenediol (490-06-2) → 3-methyl-6-(2-propyl)-1,2-benzoquinone (78617-27-3)

Guidance literature:

With sodium periodate; In dichloromethane; water; at 20 ℃; for 1h;

DOI:10.1021/acs.jnatprod.9b00339

Reference yield: 82.0%

carvacrol (499-75-2) → 3-methyl-6-(2-propyl)-1,2-benzoquinone (78617-27-3) + 3,10-dihydroxy-6,12-di-iso-propyl-3,10-dimethyltricyclo[6.2.2.02,7]dodeca-5,11-diene-4,9-dione (95475-28-8,106623-23-8,113159-72-1)

Guidance literature:

With Oxone; sodium 2-iodo-4,5-dimethylbenzenesulfonate; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; at 20 ℃; for 24h; Reagent/catalyst; Temperature; chemoselective reaction; Catalytic behavior;

DOI:10.1002/anie.201612463

Reference yield: 60.0%

carvacrol (499-75-2) → 3-methyl-6-(2-propyl)-1,2-benzoquinone (78617-27-3)

Guidance literature:

With benzeneseleninic anhydride; In tetrahydrofuran; at 50 ℃;

DOI:10.1039/P19810001473

upstream raw materials:

carvacrol

thymol

3-isopropyl-6-methyl-1,2-benzenediol