1-{[1-Cyanomethylsulfanyl-1-phenyl-meth-(Z)-ylidene]-amino}-2-methyl-pyridinium; bromide

Base Information

• Chemical Name: 1-{[1-Cyanomethylsulfanyl-1-phenyl-meth-(Z)-ylidene]-amino}-2-methyl-pyridinium; bromide
• CAS No.: 110886-34-5
• Molecular Formula: Br*C₁₅H₁₄N₃S
• Molecular Weight: 348.266
• Mol file: 110886-34-5.mol

Synonyms:1-{[1-Cyanomethylsulfanyl-1-phenyl-meth-(Z)-ylidene]-amino}-2-methyl-pyridinium; bromide

Chemical Property of 1-{[1-Cyanomethylsulfanyl-1-phenyl-meth-(Z)-ylidene]-amino}-2-methyl-pyridinium; bromide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-{[1-Cyanomethylsulfanyl-1-phenyl-meth-(Z)-ylidene]-amino}-2-methyl-pyridinium; bromide

There total 3 articles about 1-{[1-Cyanomethylsulfanyl-1-phenyl-meth-(Z)-ylidene]-amino}-2-methyl-pyridinium; bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl dithiobenzoate (2168-78-7) → 1-{[1-Cyanomethylsulfanyl-1-phenyl-meth-(Z)-ylidene]-amino}-2-methyl-pyridinium; bromide (110886-34-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 76 percent / anhydrous K₂CO₃ / ethanol / 24 h / Ambient temperature

2: CHCl₃ / Ambient temperature

With potassium carbonate; In ethanol; chloroform;

Reference yield:

1-amino-2-methylpyridinium iodide (7583-90-6) → 1-{[1-Cyanomethylsulfanyl-1-phenyl-meth-(Z)-ylidene]-amino}-2-methyl-pyridinium; bromide (110886-34-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 76 percent / anhydrous K₂CO₃ / ethanol / 24 h / Ambient temperature

2: CHCl₃ / Ambient temperature

With potassium carbonate; In ethanol; chloroform;

Reference yield:

C13H12N2S (87290-07-1) + cyanomethyl bromide (590-17-0) → 1-{[1-Cyanomethylsulfanyl-1-phenyl-meth-(Z)-ylidene]-amino}-2-methyl-pyridinium; bromide (110886-34-5)

Guidance literature:

In chloroform; Yield given; Ambient temperature;

upstream raw materials:

C₁₃H₁₂N₂S

cyanomethyl bromide

methyl dithiobenzoate

1-amino-2-methylpyridinium iodide

Downstream raw materials:

7-Methyl-2-phenyl-pyrazolo[1,5-a]pyridine-3-carbonitrile