2-trimethylsilanyl-ethanesulfonic acid {4-benzyloxy-6-benzyloxymethyl-5-[4,5-bis-benzyloxy-6-benzyloxymethyl-3-(3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-ethylsulfanyl-tetrahydro-pyran-3-yl}-amide

Base Information

Chemical Name:2-trimethylsilanyl-ethanesulfonic acid {4-benzyloxy-6-benzyloxymethyl-5-[4,5-bis-benzyloxy-6-benzyloxymethyl-3-(3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-ethylsulfanyl-tetrahydro-pyran-3-yl}-amide
CAS No.:351209-70-6
Molecular Formula:C₈₁H₉₇NO₁₅S₂Si
Molecular Weight:1416.88
Hs Code.:

2-trimethylsilanyl-ethanesulfonic acid {4-benzyloxy-6-benzyloxymethyl-5-[4,5-bis-benzyloxy-6-benzyloxymethyl-3-(3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-ethylsulfanyl-tetrahydro-pyran-3-yl}-amide

Synonyms:2-trimethylsilanyl-ethanesulfonic acid {4-benzyloxy-6-benzyloxymethyl-5-[4,5-bis-benzyloxy-6-benzyloxymethyl-3-(3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-ethylsulfanyl-tetrahydro-pyran-3-yl}-amide

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Chemical Property of 2-trimethylsilanyl-ethanesulfonic acid {4-benzyloxy-6-benzyloxymethyl-5-[4,5-bis-benzyloxy-6-benzyloxymethyl-3-(3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-ethylsulfanyl-tetrahydro-pyran-3-yl}-amide

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Technology Process of 2-trimethylsilanyl-ethanesulfonic acid {4-benzyloxy-6-benzyloxymethyl-5-[4,5-bis-benzyloxy-6-benzyloxymethyl-3-(3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-ethylsulfanyl-tetrahydro-pyran-3-yl}-amide

There total 2 articles about 2-trimethylsilanyl-ethanesulfonic acid {4-benzyloxy-6-benzyloxymethyl-5-[4,5-bis-benzyloxy-6-benzyloxymethyl-3-(3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-ethylsulfanyl-tetrahydro-pyran-3-yl}-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 125486-96-6
2-(trimethylsilyl)ethanesulfonamide

: 30383-01-8
lithium thioethoxide

: 895140-72-4
(2R,3S,4R)-4-Benzyloxy-2-benzyloxymethyl-3-[(2S,3R,4S,5S,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-3-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-3,4-dihydro-2H-pyran

: 351209-70-6
2-trimethylsilanyl-ethanesulfonic acid {4-benzyloxy-6-benzyloxymethyl-5-[4,5-bis-benzyloxy-6-benzyloxymethyl-3-(3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-ethylsulfanyl-tetrahydro-pyran-3-yl}-amide

Guidance literature:: 2-(trimethylsilyl)ethanesulfonamide; (2R,3S,4R)-4-Benzyloxy-2-benzyloxymethyl-3-[(2S,3R,4S,5S,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-3-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-3,4-dihydro-2H-pyran; With iodonium(di-γ-collidine) perchlorate;

lithium thioethoxide; In N,N-dimethyl-formamide; at -40 - 0 ℃;
DOI:10.1002/1521-3773(20010504)40:9<1728::AID-ANIE17280>3.0.CO;2-1

Reference yield:

: 2-trimethylsilanyl-ethanesulfonic acid {4-benzyloxy-6-benzyloxymethyl-5-[4,5-bis-benzyloxy-6-benzyloxymethyl-3-(3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-iodo-tetrahydro-pyran-3-yl}-amide

: 75-08-1
ethanethiol

: 351209-70-6
2-trimethylsilanyl-ethanesulfonic acid {4-benzyloxy-6-benzyloxymethyl-5-[4,5-bis-benzyloxy-6-benzyloxymethyl-3-(3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-ethylsulfanyl-tetrahydro-pyran-3-yl}-amide

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; N,N-dimethyl-formamide; at -40 - 20 ℃;
DOI:10.1016/j.tet.2006.02.080