4-Oxo-pentanoic acid (2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(4-{[bis-(4-methoxy-phenyl)-phenyl-methyl]-amino}-2-oxo-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

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Chemical Name:4-Oxo-pentanoic acid (2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(4-{[bis-(4-methoxy-phenyl)-phenyl-methyl]-amino}-2-oxo-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester
CAS No.:215117-45-6
Molecular Formula:C₅₆H₅₅N₃O₁₀
Molecular Weight:930.067
Hs Code.:

4-Oxo-pentanoic acid (2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(4-{[bis-(4-methoxy-phenyl)-phenyl-methyl]-amino}-2-oxo-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

Synonyms:4-Oxo-pentanoic acid (2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(4-{[bis-(4-methoxy-phenyl)-phenyl-methyl]-amino}-2-oxo-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

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Chemical Property of 4-Oxo-pentanoic acid (2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(4-{[bis-(4-methoxy-phenyl)-phenyl-methyl]-amino}-2-oxo-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

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Technology Process of 4-Oxo-pentanoic acid (2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(4-{[bis-(4-methoxy-phenyl)-phenyl-methyl]-amino}-2-oxo-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

There total 5 articles about 4-Oxo-pentanoic acid (2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(4-{[bis-(4-methoxy-phenyl)-phenyl-methyl]-amino}-2-oxo-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123-76-2
levulinic acid

: 80594-29-2
1-{(2R,4S,5R)-5-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-hydroxy-tetrahydro-furan-2-yl}-4-{[bis-(4-methoxy-phenyl)-phenyl-methyl]-amino}-1H-pyrimidin-2-one

: 215117-45-6
4-Oxo-pentanoic acid (2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(4-{[bis-(4-methoxy-phenyl)-phenyl-methyl]-amino}-2-oxo-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

Guidance literature:: With pyridine; dmap; dicyclohexyl-carbodiimide; In 1,4-dioxane; for 4h; Yield given; Ambient temperature;
DOI:10.1021/ja982004y

Reference yield:

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 215117-45-6
4-Oxo-pentanoic acid (2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(4-{[bis-(4-methoxy-phenyl)-phenyl-methyl]-amino}-2-oxo-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / pyridine, Et₃N, (dimethylamino)pyridine / 0.67 h / Ambient temperature

2: pyridine, (dimethylamino)pyridine, 1,3-dicyclohexylcarbodiimide / dioxane / 4 h / Ambient temperature

With pyridine; dmap; triethylamine; dicyclohexyl-carbodiimide; In 1,4-dioxane;
DOI:10.1021/ja982004y

Reference yield:

: 3992-42-5
2'-deoxycytidine monohydrochloride

: 215117-45-6
4-Oxo-pentanoic acid (2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(4-{[bis-(4-methoxy-phenyl)-phenyl-methyl]-amino}-2-oxo-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / pyridine, Et₃N, (dimethylamino)pyridine / 0.67 h / Ambient temperature

2: pyridine, (dimethylamino)pyridine, 1,3-dicyclohexylcarbodiimide / dioxane / 4 h / Ambient temperature

With pyridine; dmap; triethylamine; dicyclohexyl-carbodiimide; In 1,4-dioxane;
DOI:10.1021/ja982004y