(+/-)-N-(benzoyloxy)-1-<oxy>-3-methyl-2-butanamine

Base Information

Chemical Name:(+/-)-N-(benzoyloxy)-1-<oxy>-3-methyl-2-butanamine
CAS No.:127180-92-1
Molecular Formula:C₁₈H₃₁NO₃Si
Molecular Weight:337.535
Hs Code.:

(+/-)-N-(benzoyloxy)-1-<<dimethyl(1,1-dimethylethyl)silyl>oxy>-3-methyl-2-butanamine

Synonyms:(+/-)-N-(benzoyloxy)-1-<oxy>-3-methyl-2-butanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-N-(benzoyloxy)-1-<oxy>-3-methyl-2-butanamine

Chemical Property:

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Technology Process of (+/-)-N-(benzoyloxy)-1-<oxy>-3-methyl-2-butanamine

There total 4 articles about (+/-)-N-(benzoyloxy)-1-<oxy>-3-methyl-2-butanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 127180-91-0
(+/-)-2--3-methyl-1-butanol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 127180-92-1
(+/-)-N-(benzoyloxy)-1-<oxy>-3-methyl-2-butanamine

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; for 3.5h; Ambient temperature;
DOI:10.1021/jo00298a018

Reference yield:

: 16369-05-4,473-75-6
valinol

: 127180-92-1
(+/-)-N-(benzoyloxy)-1-<oxy>-3-methyl-2-butanamine

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / Na₂HPO₄ / tetrahydrofuran / 3 h / 25 °C

2: 87 percent / imidazole / dimethylformamide / 3.5 h / Ambient temperature

With 1H-imidazole; disodium hydrogenphosphate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo00298a018

Reference yield:

: 13893-45-3
valine ethyl ester

: 127180-92-1
(+/-)-N-(benzoyloxy)-1-<oxy>-3-methyl-2-butanamine

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / LiAlH₄

2: 56 percent / Na₂HPO₄ / tetrahydrofuran / 3 h / 25 °C

3: 87 percent / imidazole / dimethylformamide / 3.5 h / Ambient temperature

With 1H-imidazole; disodium hydrogenphosphate; lithium aluminium tetrahydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo00298a018