2-(1-(1-cyclohexyl-2-(2,4-dimethoxyphenyl)-1H-benzimidazol-5-yl)ethylidene)hydrazine carboxamide

Base Information

Chemical Name:2-(1-(1-cyclohexyl-2-(2,4-dimethoxyphenyl)-1H-benzimidazol-5-yl)ethylidene)hydrazine carboxamide
CAS No.:1383485-24-2
Molecular Formula:C₂₄H₂₉N₅O₃
Molecular Weight:435.526
Hs Code.:

Synonyms:2-(1-(1-cyclohexyl-2-(2,4-dimethoxyphenyl)-1H-benzimidazol-5-yl)ethylidene)hydrazine carboxamide

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Chemical Property of 2-(1-(1-cyclohexyl-2-(2,4-dimethoxyphenyl)-1H-benzimidazol-5-yl)ethylidene)hydrazine carboxamide

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Technology Process of 2-(1-(1-cyclohexyl-2-(2,4-dimethoxyphenyl)-1H-benzimidazol-5-yl)ethylidene)hydrazine carboxamide

There total 4 articles about 2-(1-(1-cyclohexyl-2-(2,4-dimethoxyphenyl)-1H-benzimidazol-5-yl)ethylidene)hydrazine carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1383485-16-2
1-cyclohexyl-2-(2,4-dimethoxyphenyl)-5-acetyl-1H-benzimidazole

: 563-41-7
semicarbazide hydrochloride

: 1383485-24-2
2-(1-(1-cyclohexyl-2-(2,4-dimethoxyphenyl)-1H-benzimidazol-5-yl)ethylidene)hydrazine carboxamide

Guidance literature:: With sodium acetate; In ethanol; water; for 5h; Reflux;
DOI:10.1016/j.ejmech.2012.03.038

Reference yield:

: 1368615-59-1
1-(3-amino-4-(cyclohexylamino)phenyl)ethanone

: 1383485-24-2
2-(1-(1-cyclohexyl-2-(2,4-dimethoxyphenyl)-1H-benzimidazol-5-yl)ethylidene)hydrazine carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: Oxone / water; N,N-dimethyl-formamide / 1 h / 20 °C

2: sodium acetate / ethanol; water / 5 h / Reflux

With Oxone; sodium acetate; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.03.038

Reference yield:

: 1-(4-(cyclohexylamino)-3-nitrophenyl)ethanone

: 1383485-24-2
2-(1-(1-cyclohexyl-2-(2,4-dimethoxyphenyl)-1H-benzimidazol-5-yl)ethylidene)hydrazine carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / ethanol / 2 h / 20 °C

2: Oxone / water; N,N-dimethyl-formamide / 1 h / 20 °C

3: sodium acetate / ethanol; water / 5 h / Reflux

With Oxone; palladium 10% on activated carbon; hydrogen; sodium acetate; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.03.038