5,6-dihydro-5-benzyloxycarbonylaminoacetyl-4-ethoxycarbonyl-4H-pyrrolo<1,2-a><1,4>benzodiazepine

Base Information

Chemical Name:5,6-dihydro-5-benzyloxycarbonylaminoacetyl-4-ethoxycarbonyl-4H-pyrrolo<1,2-a><1,4>benzodiazepine
CAS No.:122485-07-8
Molecular Formula:C₂₅H₂₅N₃O₅
Molecular Weight:447.491
Hs Code.:

Synonyms:5,6-dihydro-5-benzyloxycarbonylaminoacetyl-4-ethoxycarbonyl-4H-pyrrolo<1,2-a><1,4>benzodiazepine

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Chemical Property of 5,6-dihydro-5-benzyloxycarbonylaminoacetyl-4-ethoxycarbonyl-4H-pyrrolo<1,2-a><1,4>benzodiazepine

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 5,6-dihydro-5-benzyloxycarbonylaminoacetyl-4-ethoxycarbonyl-4H-pyrrolo<1,2-a><1,4>benzodiazepine

There total 2 articles about 5,6-dihydro-5-benzyloxycarbonylaminoacetyl-4-ethoxycarbonyl-4H-pyrrolo<1,2-a><1,4>benzodiazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 122485-06-7
5,6-dihydro-4-ethoxycarbonyl-4H-pyrrolo<1,2-a><1,4>benzodiazepine

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

: 122485-07-8
5,6-dihydro-5-benzyloxycarbonylaminoacetyl-4-ethoxycarbonyl-4H-pyrrolo<1,2-a><1,4>benzodiazepine

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; 1.) 0-5 deg C, 1 h; 2.) r.t., 4 h;
DOI:10.1016/S0040-4020(01)80106-X

Reference yield:

: 33265-72-4
1-(2-aminomethylphenyl)-1H-pyrroloe hydrochloride

: 122485-07-8
5,6-dihydro-5-benzyloxycarbonylaminoacetyl-4-ethoxycarbonyl-4H-pyrrolo<1,2-a><1,4>benzodiazepine

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / ethanol / 5 h / Heating

2: 98 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride / CH₂Cl₂ / 1.) 0-5 deg C, 1 h; 2.) r.t., 4 h

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In ethanol; dichloromethane;
DOI:10.1016/S0040-4020(01)80106-X

Reference yield: 50.0%

: 122485-07-8
5,6-dihydro-5-benzyloxycarbonylaminoacetyl-4-ethoxycarbonyl-4H-pyrrolo<1,2-a><1,4>benzodiazepine

: 122485-08-9
3b,4,6,7-tetrahydro-4,7-dioxo-5H,9H-pyrazino<2,1-c>pyrrolo<1,2-a><1,4>benzodiazepine

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; at 50 ℃; for 6h; under 3040 Torr;
DOI:10.1016/S0040-4020(01)80106-X