1-Phenyl-1-nitroaceton

Base Information

• Chemical Name: 1-Phenyl-1-nitroaceton
• CAS No.: 26226-65-3
• Molecular Formula: C₉H₉NO₃
• Molecular Weight: 179.175
• Mol file: 26226-65-3.mol

Synonyms:1-Phenyl-1-nitroaceton

Chemical Property of 1-Phenyl-1-nitroaceton

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Phenyl-1-nitroaceton

There total 1 articles about 1-Phenyl-1-nitroaceton which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

2-methyl-2-nitro-3-phenyloxirane (22596-45-8) → 1-Phenyl-1-nitroaceton (26226-65-3)

Guidance literature:

With clay; potassium bromide; In benzene; for 0.25h; Ambient temperature;

DOI:10.1002/jhet.5570340638

Reference yield: 75.0%

1-Phenyl-1-nitroaceton (26226-65-3) + allyl alcohol (107-18-6) + cinnamyl tert-butyl carbonate (124517-47-1) → C19H19NO2

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In dichloromethane; 1,2-dichloro-ethane; at 80 ℃;

DOI:10.1002/anie.201006273

Reference yield:

1-Phenyl-1-nitroaceton (26226-65-3) → 1-phenyl-propane-1,2-dione 1-oxime (25355-34-4)

Guidance literature:

With isopropyl alcohol; Irradiation;

DOI:10.1246/bcsj.46.3198

upstream raw materials:

2-methyl-2-nitro-3-phenyloxirane

Downstream raw materials:

1-phenyl-propane-1,2-dione 1-oxime