(E)-N-(3-methoxy-6-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridine-2-yl)methanesulfonamide

Base Information

Chemical Name:(E)-N-(3-methoxy-6-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridine-2-yl)methanesulfonamide
CAS No.:1353547-89-3
Molecular Formula:C₁₉H₂₄N₂O₈S₂
Molecular Weight:472.54
Hs Code.:

Synonyms:(E)-N-(3-methoxy-6-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridine-2-yl)methanesulfonamide

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Chemical Property of (E)-N-(3-methoxy-6-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridine-2-yl)methanesulfonamide

Chemical Property:

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Technology Process of (E)-N-(3-methoxy-6-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridine-2-yl)methanesulfonamide

There total 8 articles about (E)-N-(3-methoxy-6-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridine-2-yl)methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1353547-84-8
(E)-3-methoxy-6-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-2-amine

: 124-63-0
methanesulfonyl chloride

: 1353547-89-3
(E)-N-(3-methoxy-6-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridine-2-yl)methanesulfonamide

Guidance literature:: With pyridine; at 0 - 20 ℃; for 14h;
DOI:10.1021/jm4019614

Reference yield:

: 6-(bromomethyl)-3-methoxy-2-nitropyridine

: 1353547-89-3
(E)-N-(3-methoxy-6-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridine-2-yl)methanesulfonamide

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium carbonate / methanol / 10 h / 20 °C

2.1: dihydrogen peroxide; acetic acid / 7 h / 50 °C

3.1: water; sodium carbonate / methanol / 10 h / 20 °C

3.2: pH 2

4.1: acetic anhydride / toluene / 5 h / Reflux

5.1: acetic acid; iron / methanol / 3 h / 50 °C / Inert atmosphere

6.1: pyridine / 20 °C / Cooling with ice

With pyridine; water; dihydrogen peroxide; acetic anhydride; iron; sodium carbonate; potassium carbonate; acetic acid; In methanol; toluene;

Reference yield:

: 24015-98-3
3-methoxy-6-methyl-2-nitro-pyridine

: 1353547-89-3
(E)-N-(3-methoxy-6-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridine-2-yl)methanesulfonamide

Guidance literature:: Multi-step reaction with 7 steps

1.1: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane / 56 h / Inert atmosphere; Reflux

2.1: potassium carbonate / methanol / 10 h / 20 °C

3.1: dihydrogen peroxide; acetic acid / 7 h / 50 °C

4.1: water; sodium carbonate / methanol / 10 h / 20 °C

4.2: pH 2

5.1: acetic anhydride / toluene / 5 h / Reflux

6.1: acetic acid; iron / methanol / 3 h / 50 °C / Inert atmosphere

7.1: pyridine / 20 °C / Cooling with ice

With pyridine; N-Bromosuccinimide; water; dihydrogen peroxide; acetic anhydride; iron; sodium carbonate; potassium carbonate; acetic acid; dibenzoyl peroxide; In methanol; tetrachloromethane; toluene;