(E)-3-methoxy-6-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-2-amine

Base Information

Chemical Name:(E)-3-methoxy-6-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-2-amine
CAS No.:1353547-84-8
Molecular Formula:C₁₈H₂₂N₂O₆S
Molecular Weight:394.448
Hs Code.:

Synonyms:(E)-3-methoxy-6-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-2-amine

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Chemical Property of (E)-3-methoxy-6-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-2-amine

Chemical Property:

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Technology Process of (E)-3-methoxy-6-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-2-amine

There total 7 articles about (E)-3-methoxy-6-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1353547-83-7
(E)-3-methoxy-2-nitro-6-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridine

: 1353547-84-8
(E)-3-methoxy-6-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-2-amine

Guidance literature:: With iron; acetic acid; In methanol; at 50 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jm4019614

Reference yield:

: 6-(bromomethyl)-3-methoxy-2-nitropyridine

: 1353547-84-8
(E)-3-methoxy-6-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-2-amine

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / methanol / 10 h / 20 °C

2.1: dihydrogen peroxide; acetic acid / 7 h / 50 °C

3.1: water; sodium carbonate / methanol / 10 h / 20 °C

3.2: pH 2

4.1: acetic anhydride / toluene / 5 h / Reflux

5.1: acetic acid; iron / methanol / 3 h / 50 °C / Inert atmosphere

With water; dihydrogen peroxide; acetic anhydride; iron; sodium carbonate; potassium carbonate; acetic acid; In methanol; toluene;

Reference yield:

: 24015-98-3
3-methoxy-6-methyl-2-nitro-pyridine

: 1353547-84-8
(E)-3-methoxy-6-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-2-amine

Guidance literature:: Multi-step reaction with 6 steps

1.1: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane / 56 h / Inert atmosphere; Reflux

2.1: potassium carbonate / methanol / 10 h / 20 °C

3.1: dihydrogen peroxide; acetic acid / 7 h / 50 °C

4.1: water; sodium carbonate / methanol / 10 h / 20 °C

4.2: pH 2

5.1: acetic anhydride / toluene / 5 h / Reflux

6.1: acetic acid; iron / methanol / 3 h / 50 °C / Inert atmosphere

With N-Bromosuccinimide; water; dihydrogen peroxide; acetic anhydride; iron; sodium carbonate; potassium carbonate; acetic acid; dibenzoyl peroxide; In methanol; tetrachloromethane; toluene;