ethyl 3-oxo-2-[4-oxo-3-phenyl(1,3-thiazolidin-2-ylidene)]-3-phenylpropanoate

Base Information

Chemical Name:ethyl 3-oxo-2-[4-oxo-3-phenyl(1,3-thiazolidin-2-ylidene)]-3-phenylpropanoate
CAS No.:758696-42-3
Molecular Formula:C₂₀H₁₇NO₄S
Molecular Weight:367.425
Hs Code.:

Synonyms:ethyl 3-oxo-2-[4-oxo-3-phenyl(1,3-thiazolidin-2-ylidene)]-3-phenylpropanoate

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Chemical Property of ethyl 3-oxo-2-[4-oxo-3-phenyl(1,3-thiazolidin-2-ylidene)]-3-phenylpropanoate

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Technology Process of ethyl 3-oxo-2-[4-oxo-3-phenyl(1,3-thiazolidin-2-ylidene)]-3-phenylpropanoate

There total 4 articles about ethyl 3-oxo-2-[4-oxo-3-phenyl(1,3-thiazolidin-2-ylidene)]-3-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 94-02-0
ethyl 3-oxo-3-phenylpropionate

: 103-72-0
phenyl isothiocyanate

: 79-04-9
chloroacetyl chloride

: 758696-42-3
ethyl 3-oxo-2-[4-oxo-3-phenyl(1,3-thiazolidin-2-ylidene)]-3-phenylpropanoate

Guidance literature:: ethyl 3-oxo-3-phenylpropionate; phenyl isothiocyanate; With potassium hydroxide; In N,N-dimethyl-formamide; at 20 ℃; for 3h;

chloroacetyl chloride; In N,N-dimethyl-formamide; for 2h;
DOI:10.1002/hc.10222

Reference yield: 79.0%

: 758696-40-1
ethyl (2Z)-3-[(ethoxycarbonyl)methylthio]-3-(phenylamino)-2-(phenylcarbonyl)prop-2-enoate

: 758696-42-3
ethyl 3-oxo-2-[4-oxo-3-phenyl(1,3-thiazolidin-2-ylidene)]-3-phenylpropanoate

Guidance literature:: With sulfuric acid; at 20 ℃; for 1h;
DOI:10.1002/hc.10222

Reference yield:

: 94-02-0
ethyl 3-oxo-3-phenylpropionate

: 758696-42-3
ethyl 3-oxo-2-[4-oxo-3-phenyl(1,3-thiazolidin-2-ylidene)]-3-phenylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / potassium hydroxide / dimethylformamide / 5 h / 20 °C

2: 79 percent / conc. sulfuric acid / 1 h / 20 °C

With potassium hydroxide; sulfuric acid; In N,N-dimethyl-formamide;
DOI:10.1002/hc.10222