5-benzyloxycarbonylamino-6-oxo-2-(pyridin-3-yl)-1,6-dihydro-1-pyrimidinylacetaldehyde dimethyl acetal

Base Information

Chemical Name:5-benzyloxycarbonylamino-6-oxo-2-(pyridin-3-yl)-1,6-dihydro-1-pyrimidinylacetaldehyde dimethyl acetal
CAS No.:148747-93-7
Molecular Formula:C₂₁H₂₂N₄O₅
Molecular Weight:410.429
Hs Code.:

Synonyms:5-benzyloxycarbonylamino-6-oxo-2-(pyridin-3-yl)-1,6-dihydro-1-pyrimidinylacetaldehyde dimethyl acetal

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Chemical Property of 5-benzyloxycarbonylamino-6-oxo-2-(pyridin-3-yl)-1,6-dihydro-1-pyrimidinylacetaldehyde dimethyl acetal

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Technology Process of 5-benzyloxycarbonylamino-6-oxo-2-(pyridin-3-yl)-1,6-dihydro-1-pyrimidinylacetaldehyde dimethyl acetal

There total 4 articles about 5-benzyloxycarbonylamino-6-oxo-2-(pyridin-3-yl)-1,6-dihydro-1-pyrimidinylacetaldehyde dimethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4129-17-3
diphenylphosphoranyl azide

: 148747-92-6
methyl 1-(2,2-dimethoxyethyl)-2-(3-pyridyl)pyrimidin-6(1H)-one-5-carboxylate

: 148747-93-7
5-benzyloxycarbonylamino-6-oxo-2-(pyridin-3-yl)-1,6-dihydro-1-pyrimidinylacetaldehyde dimethyl acetal

Guidance literature:: With triethylamine; lithium iodide; benzyl alcohol; In 1,4-dioxane; pyridine; ethyl acetate; toluene;

Reference yield:

: 148747-91-5
N-(2,2-dimethoxyethyl)-3-pyridinecarboxamidine

: 148747-93-7
5-benzyloxycarbonylamino-6-oxo-2-(pyridin-3-yl)-1,6-dihydro-1-pyrimidinylacetaldehyde dimethyl acetal

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 1.5 h / 100 °C

2: pyridine, lithium iodide / 2 h / Heating

3: 1.) Et₃N, diphenyl phosphorazidate / 1.) 100 deg C, 2 h, 2.) 100 deg C, 12 h

With pyridine; diphenyl phosphoryl azide; triethylamine; lithium iodide; In methanol;
DOI:10.1021/jm00001a015

Reference yield:

: Nicotinimidoyl chloride; hydrochloride

: 148747-93-7
5-benzyloxycarbonylamino-6-oxo-2-(pyridin-3-yl)-1,6-dihydro-1-pyrimidinylacetaldehyde dimethyl acetal

Guidance literature:: Multi-step reaction with 4 steps

1: methanol / 72 h / 5 °C

2: methanol / 1.5 h / 100 °C

3: pyridine, lithium iodide / 2 h / Heating

4: 1.) Et₃N, diphenyl phosphorazidate / 1.) 100 deg C, 2 h, 2.) 100 deg C, 12 h

With pyridine; diphenyl phosphoryl azide; triethylamine; lithium iodide; In methanol;
DOI:10.1021/jm00001a015