{(SO3CF3)(H2O)(α,α,α,α-tetrakis(o-pivalamidophenyl)porphinato)iron(III)}

Base Information

Chemical Name:{(SO3CF3)(H2O)(α,α,α,α-tetrakis(o-pivalamidophenyl)porphinato)iron(III)}
CAS No.:124442-29-1
Molecular Formula:C₆₅H₆₆F₃FeN₈O₈S
Molecular Weight:1232.2
Hs Code.:

Synonyms:{(SO3CF3)(H2O)(α,α,α,α-tetrakis(o-pivalamidophenyl)porphinato)iron(III)}

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Chemical Property of {(SO3CF3)(H2O)(α,α,α,α-tetrakis(o-pivalamidophenyl)porphinato)iron(III)}

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Technology Process of {(SO3CF3)(H2O)(α,α,α,α-tetrakis(o-pivalamidophenyl)porphinato)iron(III)}

There total 1 articles about {(SO3CF3)(H2O)(α,α,α,α-tetrakis(o-pivalamidophenyl)porphinato)iron(III)} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 105118-92-1,92078-42-7,87334-91-6,86107-94-0,87334-93-8,87334-92-7,104486-25-1
chloroiron(III) meso-α,α,α,α-tetrakis(o-pivalamidophenyl)porphyrinate

: 2923-28-6
silver trifluoromethanesulfonate

: 124442-29-1
{(SO3CF3)(H2O)(α,α,α,α-tetrakis(o-pivalamidophenyl)porphinato)iron(III)}

Guidance literature:: In tetrahydrofuran; soln. of silver triflate addn. to soln. of Fe-complex; stirring (Ar, 12 h, room temp.); filtraqtion, hexane addn. (swirling), soln. concn. (vac.) on pptn.;

Reference yield:

: 124442-29-1
{(SO3CF3)(H2O)(α,α,α,α-tetrakis(o-pivalamidophenyl)porphinato)iron(III)}

: 52629-13-7,126783-80-0,83198-46-3
tetra(α,α,α,α-orthopivalamide)phenylporphyrinatoiron(II)

Guidance literature:: With zinc amalgam; In chlorobenzene; (inert atm.); stirring (1 h); filtn.;
DOI:10.1021/ja963871a

Reference yield:

: 7758-09-0
potassium nitrite

: 124442-29-1
{(SO3CF3)(H2O)(α,α,α,α-tetrakis(o-pivalamidophenyl)porphinato)iron(III)}

: 23978-09-8
[2.2.2]cryptande

: K⁽¹⁺⁾*C₁₈H₃₆N₂O₆*FeC₂₀H₈N₄(C₆H₄NHCOC(CH₃)3)4NO₂^(1-)*H₂O*C₆H₅Cl=K(C₁₈H₃₆N₂O₆)FeC₂₀H₈N₄(C₆H₄NHCOC(CH₃)3)4(NO₂)*H₂O*C₆H₅Cl

Guidance literature:: With Zn amalgam; C₆H₅Cl; H₂O; In chlorobenzene; a mixt. of complex and Zn amalgam were stirred for 1 h under Ar in C6H5Cl, the soln. was filtered into a soln. was made by stirring overnight Kryptofix-222 and KNO2 in C6H5Cl; the soln. was filtered, crystals were prepared by slow diffusion of pentane into the chlorobenzene soln.;
DOI:10.1021/ja000149a