6,6-dimethyl-3-oxocyclohex-1-en-1-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

Base Information

Chemical Name:6,6-dimethyl-3-oxocyclohex-1-en-1-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate
CAS No.:1396274-95-5
Molecular Formula:C₁₂H₁₁F₉O₄S
Molecular Weight:422.269
Hs Code.:

Synonyms:6,6-dimethyl-3-oxocyclohex-1-en-1-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

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Chemical Property of 6,6-dimethyl-3-oxocyclohex-1-en-1-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

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Technology Process of 6,6-dimethyl-3-oxocyclohex-1-en-1-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

There total 2 articles about 6,6-dimethyl-3-oxocyclohex-1-en-1-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 6,6-dimethylcyclohex-1-en-1-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

: 1396274-95-5
6,6-dimethyl-3-oxocyclohex-1-en-1-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

Guidance literature:: With tert.-butylhydroperoxide; iron(III) chloride; In water; acetonitrile; at 40 ℃; for 24h; regioselective reaction; Sealed tube;
DOI:10.1021/acs.orglett.9b00845

Reference yield: 54.0%

: 375-72-4
Nonafluorobutanesulfonyl fluoride

: 562-46-9
4,4-dimethylcyclohexane-1,3-dione

: 999-97-3
1,1,1,3,3,3-hexamethyl-disilazane

: 1396274-95-5
6,6-dimethyl-3-oxocyclohex-1-en-1-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

: 1396274-92-2
C₁₂H₁₁F₉O₄S

Guidance literature:: 4,4-dimethylcyclohexane-1,3-dione; 1,1,1,3,3,3-hexamethyl-disilazane; With 1H-imidazole; at 20 - 130 ℃; for 3h; Inert atmosphere;

With cesium fluoride; In tetrahydrofuran; at 0 ℃; for 0.166667h; Inert atmosphere;

Nonafluorobutanesulfonyl fluoride; In tetrahydrofuran; at 0 - 20 ℃; for 18h; Inert atmosphere;
DOI:10.1055/s-0031-1290945