[(o-MeOC₆H₄)CH₂]2SnCl₂

Base Information

• Chemical Name: [(o-MeOC₆H₄)CH₂]2SnCl₂
• CAS No.: 622863-77-8
• Molecular Formula: C₁₆H₁₈Cl₂O₂Sn
• Molecular Weight: 431.934
• Mol file: 622863-77-8.mol

Synonyms:[(o-MeOC₆H₄)CH₂]2SnCl₂

Chemical Property of [(o-MeOC₆H₄)CH₂]2SnCl₂

Chemical Property:

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Technology Process of [(o-MeOC₆H₄)CH₂]2SnCl₂

There total 1 articles about [(o-MeOC₆H₄)CH₂]2SnCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

tin (7440-31-5) + o-Methoxybenzyl chloride (7035-02-1) → [(o-MeOC6H4)CH2]2SnCl2 (622863-77-8)

Guidance literature:

With water; In toluene; (N2) mixt Sn and water was suspended in toluene and heated in boiling water bath, benzyl chloride was added and refluxed for 4 h; soln. was cooled and filtered, solvent was removed in vacuo, residue wascrystd. from hexane at -20°C; elem. anal.;

DOI:10.1021/ic901800c

upstream raw materials:

tin

o-Methoxybenzyl chloride