cyclohexyl 3,4,6-tri-O-benzyl-2-O-(2,2-dimethyltrimethylene phosphonoyl)-β-D-glucopyranoside

Base Information

Chemical Name:cyclohexyl 3,4,6-tri-O-benzyl-2-O-(2,2-dimethyltrimethylene phosphonoyl)-β-D-glucopyranoside
CAS No.:906360-08-5
Molecular Formula:C₃₈H₄₉O₉P
Molecular Weight:680.775
Hs Code.:

Synonyms:cyclohexyl 3,4,6-tri-O-benzyl-2-O-(2,2-dimethyltrimethylene phosphonoyl)-β-D-glucopyranoside

Suppliers and Price of cyclohexyl 3,4,6-tri-O-benzyl-2-O-(2,2-dimethyltrimethylene phosphonoyl)-β-D-glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of cyclohexyl 3,4,6-tri-O-benzyl-2-O-(2,2-dimethyltrimethylene phosphonoyl)-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of cyclohexyl 3,4,6-tri-O-benzyl-2-O-(2,2-dimethyltrimethylene phosphonoyl)-β-D-glucopyranoside

There total 4 articles about cyclohexyl 3,4,6-tri-O-benzyl-2-O-(2,2-dimethyltrimethylene phosphonoyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 906360-08-5
cyclohexyl 3,4,6-tri-O-benzyl-2-O-(2,2-dimethyltrimethylene phosphonoyl)-β-D-glucopyranoside

Guidance literature:

Reference yield:

: 906360-00-7
phenyl 3,4,6-tri-O-benzyl-2-O-(2,2-dimethyltrimethylene phosphonoyl)-β-D-thioglucopyranoside

: 108-93-0
cyclohexanol

: 906360-08-5
cyclohexyl 3,4,6-tri-O-benzyl-2-O-(2,2-dimethyltrimethylene phosphonoyl)-β-D-glucopyranoside

Guidance literature:: With N-iodo-succinimide; 4 A molecular sieve; In dichloromethane; at -40 ℃; for 1h;
DOI:10.1002/anie.200602699

Reference yield:

: 4090-55-5
2-chloro-5,5-dimethyl[1,3,2]dioxaphosphinane 2-oxide

: 906360-08-5
cyclohexyl 3,4,6-tri-O-benzyl-2-O-(2,2-dimethyltrimethylene phosphonoyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / NaH / various solvent(s); tetrahydrofuran / 2.5 h / 20 °C

2: 79 percent Spectr_. / N-iodosuccinimide; molecular sieves 4 Angstroem / CH₂Cl₂ / 1 h / -40 °C

With N-iodo-succinimide; 4 A molecular sieve; sodium hydride; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.200602699