phenyl 3,4,6-tri-O-benzyl-2-O-(2,2-dimethyltrimethylene phosphonoyl)-β-D-thioglucopyranoside

Base Information

Chemical Name:phenyl 3,4,6-tri-O-benzyl-2-O-(2,2-dimethyltrimethylene phosphonoyl)-β-D-thioglucopyranoside
CAS No.:906360-00-7
Molecular Formula:C₃₈H₄₃O₈PS
Molecular Weight:690.794
Hs Code.:

Synonyms:phenyl 3,4,6-tri-O-benzyl-2-O-(2,2-dimethyltrimethylene phosphonoyl)-β-D-thioglucopyranoside

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Chemical Property of phenyl 3,4,6-tri-O-benzyl-2-O-(2,2-dimethyltrimethylene phosphonoyl)-β-D-thioglucopyranoside

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Technology Process of phenyl 3,4,6-tri-O-benzyl-2-O-(2,2-dimethyltrimethylene phosphonoyl)-β-D-thioglucopyranoside

There total 2 articles about phenyl 3,4,6-tri-O-benzyl-2-O-(2,2-dimethyltrimethylene phosphonoyl)-β-D-thioglucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 906360-00-7
phenyl 3,4,6-tri-O-benzyl-2-O-(2,2-dimethyltrimethylene phosphonoyl)-β-D-thioglucopyranoside

Guidance literature:

Reference yield:

: 126-30-7
2,2-Dimethyl-1,3-propanediol

: 906360-00-7
phenyl 3,4,6-tri-O-benzyl-2-O-(2,2-dimethyltrimethylene phosphonoyl)-β-D-thioglucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / phosphorus oxychloride; triethylamine / CH₂Cl₂ / 0.5 h / 0 °C

2: 94 percent / NaH / various solvent(s); tetrahydrofuran / 2.5 h / 20 °C

With sodium hydride; triethylamine; trichlorophosphate; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.200602699

Reference yield: 71.0%

: 874364-55-3
C₂₉H₂₃O₇NCl₄S

: 906360-00-7
phenyl 3,4,6-tri-O-benzyl-2-O-(2,2-dimethyltrimethylene phosphonoyl)-β-D-thioglucopyranoside

: C₆₁H₆₀O₁₅NCl₄PS

Guidance literature:: phenyl 3,4,6-tri-O-benzyl-2-O-(2,2-dimethyltrimethylene phosphonoyl)-β-D-thioglucopyranoside; With 2,6-di-tert-butyl-4-methylpyridine; 1-(phenylsulphenyl)piperidylamide; trifluoromethylsulfonic anhydride; In dichloromethane; at -60 ℃;

C₂₉H₂₃O₇NCl₄S; In dichloromethane; at -60 ℃; Further stages.;
DOI:10.1002/anie.200602699