2-cyclopropyl-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylacrylamide

Base Information

Chemical Name:2-cyclopropyl-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylacrylamide
CAS No.:1068601-84-2
Molecular Formula:C₁₆H₂₁NO₂
Molecular Weight:259.348
Hs Code.:

Synonyms:2-cyclopropyl-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylacrylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-cyclopropyl-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylacrylamide

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Technology Process of 2-cyclopropyl-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylacrylamide

There total 1 articles about 2-cyclopropyl-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylacrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1068601-82-0
C₁₇H₂₅NO₅S

: 1068601-84-2
2-cyclopropyl-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylacrylamide

Guidance literature:: With sodium methylate; In methanol; at 23 ℃; Inert atmosphere; Reflux;
DOI:10.1021/ja806021y

Reference yield: 92.0%

: 1068601-84-2
2-cyclopropyl-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylacrylamide

: 591-51-5
phenyllithium

: 74-88-4
methyl iodide

: 1068602-45-8
(S)-2-cyclopropyl-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N,2-dimethyl-3-phenylpropanamide

Guidance literature:: 2-cyclopropyl-N-[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]-N-methylacrylamide; phenyllithium; With lithium chloride; In tetrahydrofuran; dibutyl ether; at -78 - 0 ℃; Inert atmosphere;

methyl iodide; In tetrahydrofuran; dibutyl ether; at 0 ℃; for 2h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ja806021y