Technology Process of C23H35N3O5
There total 10 articles about C23H35N3O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 92 percent / m-chloroperoxybenzoic acid / CH2Cl2 / 18 h / 20 °C
2.1: ethanol / 6 h / Heating
2.2: 27 percent / CHCl3 / 6 h / 20 °C
3.1: 82 percent / pyridine*SO3; Et3N / dimethylsulfoxide / 3 h / 5 °C
4.1: 81 percent / NaHCO3; HONH2*HCl / ethanol; tetrahydrofuran / 1 h / 40 °C
5.1: TBAB; aq. NaOH / CH2Cl2 / 5 h / 20 °C
With
sodium hydroxide; hydroxylamine hydrochloride; tetrabutylammomium bromide; sulfur trioxide pyridine complex; sodium hydrogencarbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; ethanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1016/j.bmcl.2007.05.093
- Guidance literature:
-
With
sodium hydroxide; tetrabutylammomium bromide;
In
dichloromethane;
at 20 ℃;
for 5h;
DOI:10.1016/j.bmcl.2007.05.093
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: CHCl3 / 12 h / 20 °C
2.1: 92 percent / m-chloroperoxybenzoic acid / CH2Cl2 / 18 h / 20 °C
3.1: ethanol / 6 h / Heating
3.2: 27 percent / CHCl3 / 6 h / 20 °C
4.1: 82 percent / pyridine*SO3; Et3N / dimethylsulfoxide / 3 h / 5 °C
5.1: 81 percent / NaHCO3; HONH2*HCl / ethanol; tetrahydrofuran / 1 h / 40 °C
6.1: TBAB; aq. NaOH / CH2Cl2 / 5 h / 20 °C
With
sodium hydroxide; hydroxylamine hydrochloride; tetrabutylammomium bromide; sulfur trioxide pyridine complex; sodium hydrogencarbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; ethanol; dichloromethane; chloroform; dimethyl sulfoxide;
DOI:10.1016/j.bmcl.2007.05.093