Technology Process of C27H18FN
There total 3 articles about C27H18FN which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
1,2-dimethoxyethane; water;
for 4h;
Reflux;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogenchloride; potassium iodide; iodic acid / water; methanol / 20 °C
2: sulfuric acid; acetic acid / 5 h / 120 °C
3: potassium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 4 h / Reflux; Inert atmosphere
With
hydrogenchloride; sulfuric acid; iodic acid; potassium carbonate; acetic acid; potassium iodide;
tetrakis(triphenylphosphine) palladium(0);
In
methanol; 1,2-dimethoxyethane; water;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sulfuric acid; acetic acid / 5 h / 120 °C
2: potassium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 4 h / Reflux; Inert atmosphere
With
sulfuric acid; potassium carbonate; acetic acid;
tetrakis(triphenylphosphine) palladium(0);
In
1,2-dimethoxyethane; water;