benzamido-methoxycarbonylethyl-4,7-bis-(ethoxycarbonylmethyl)-1,4,7-triaza cyclononane

Base Information

Chemical Name:benzamido-methoxycarbonylethyl-4,7-bis-(ethoxycarbonylmethyl)-1,4,7-triaza cyclononane
CAS No.:1609973-73-0
Molecular Formula:C₂₅H₃₈N₄O₇
Molecular Weight:506.599
Hs Code.:

Synonyms:benzamido-methoxycarbonylethyl-4,7-bis-(ethoxycarbonylmethyl)-1,4,7-triaza cyclononane

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Chemical Property of benzamido-methoxycarbonylethyl-4,7-bis-(ethoxycarbonylmethyl)-1,4,7-triaza cyclononane

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Technology Process of benzamido-methoxycarbonylethyl-4,7-bis-(ethoxycarbonylmethyl)-1,4,7-triaza cyclononane

There total 4 articles about benzamido-methoxycarbonylethyl-4,7-bis-(ethoxycarbonylmethyl)-1,4,7-triaza cyclononane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: benzamido-methoxycarbonylethyl-1,4,7-triaza cyclononane

: 105-36-2
ethyl bromoacetate

: 1609973-73-0
benzamido-methoxycarbonylethyl-4,7-bis-(ethoxycarbonylmethyl)-1,4,7-triaza cyclononane

Guidance literature:: With potassium carbonate; In acetonitrile; at 20 ℃; for 2.5h;
DOI:10.1039/c4dt00386a

Reference yield:

: 257955-17-2
Bz-ΔAla(N-Boc)-OMe

: 1609973-73-0
benzamido-methoxycarbonylethyl-4,7-bis-(ethoxycarbonylmethyl)-1,4,7-triaza cyclononane

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / 3 h / 20 °C

2: trifluoroacetic acid / dichloromethane / 20 °C

3: potassium carbonate / acetonitrile / 2.5 h / 20 °C

With potassium carbonate; trifluoroacetic acid; In dichloromethane; acetonitrile; 1: |Michael Addition;
DOI:10.1039/c4dt00386a

Reference yield:

: 1609973-70-7
N-tert-butoxycarbonylbenzamido-methoxycarbonylethyl-1,4,7-triaza cyclononane

: 1609973-73-0
benzamido-methoxycarbonylethyl-4,7-bis-(ethoxycarbonylmethyl)-1,4,7-triaza cyclononane

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 20 °C

2: potassium carbonate / acetonitrile / 2.5 h / 20 °C

With potassium carbonate; trifluoroacetic acid; In dichloromethane; acetonitrile;
DOI:10.1039/c4dt00386a