N-(1-(dimethyl(phenyl)silyl)-1-phenylethyl)-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-(1-(dimethyl(phenyl)silyl)-1-phenylethyl)-4-methylbenzenesulfonamide
CAS No.:1283154-36-8
Molecular Formula:C₂₃H₂₇NO₂SSi
Molecular Weight:409.624
Hs Code.:

Synonyms:N-(1-(dimethyl(phenyl)silyl)-1-phenylethyl)-4-methylbenzenesulfonamide

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Chemical Property of N-(1-(dimethyl(phenyl)silyl)-1-phenylethyl)-4-methylbenzenesulfonamide

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Technology Process of N-(1-(dimethyl(phenyl)silyl)-1-phenylethyl)-4-methylbenzenesulfonamide

There total 13 articles about N-(1-(dimethyl(phenyl)silyl)-1-phenylethyl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1379506-16-7
C₂₂H₂₃NO₂SSi

: 75-16-1
methylmagnesium bromide

: 1283154-36-8
N-(1-(dimethyl(phenyl)silyl)-1-phenylethyl)-4-methylbenzenesulfonamide

Guidance literature:: In tetrahydrofuran; diethyl ether; at -78 - 70 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol301194e

Reference yield: 90.0%

: 1379506-15-6
C₂₃H₂₇NO₃SSi

: 75-16-1
methylmagnesium bromide

: 1283154-36-8
N-(1-(dimethyl(phenyl)silyl)-1-phenylethyl)-4-methylbenzenesulfonamide

Guidance literature:: In tetrahydrofuran; diethyl ether; at -78 - 70 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol301194e

Reference yield: 86.0%

: 3839-31-4
dimethyl(phenyl)silyl lithium

: 22158-84-5
N-(p-Toluolsulfonyl)-benzimidsaeure-methylester

: 75-16-1
methylmagnesium bromide

: 1283154-36-8
N-(1-(dimethyl(phenyl)silyl)-1-phenylethyl)-4-methylbenzenesulfonamide

Guidance literature:: dimethyl(phenyl)silyl lithium; N-(p-Toluolsulfonyl)-benzimidsaeure-methylester; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

methylmagnesium bromide; In tetrahydrofuran; at -78 - -45 ℃; for 2.5h; Inert atmosphere;
DOI:10.1021/ol301194e