9-deoxo-9a-{N'-[4-(aminosulfonyl)phenyl]carbamoyl}-9a-aza-9a-homoerythromycin

Base Information

Chemical Name:9-deoxo-9a-{N'-[4-(aminosulfonyl)phenyl]carbamoyl}-9a-aza-9a-homoerythromycin
CAS No.:690258-32-3
Molecular Formula:C₄₄H₇₆N₄O₁₅S
Molecular Weight:933.171
Hs Code.:

Synonyms:9-deoxo-9a-{N'-[4-(aminosulfonyl)phenyl]carbamoyl}-9a-aza-9a-homoerythromycin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-deoxo-9a-{N'-[4-(aminosulfonyl)phenyl]carbamoyl}-9a-aza-9a-homoerythromycin

Chemical Property:

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Technology Process of 9-deoxo-9a-{N'-[4-(aminosulfonyl)phenyl]carbamoyl}-9a-aza-9a-homoerythromycin

There total 4 articles about 9-deoxo-9a-{N'-[4-(aminosulfonyl)phenyl]carbamoyl}-9a-aza-9a-homoerythromycin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 9-deoxo-9-dihydro-9a-aza-9a-homoerithromycin A

: 6752-38-1
4-chlorosulfonylbenzene isocyanate

: 690258-32-3
9-deoxo-9a-{N'-[4-(aminosulfonyl)phenyl]carbamoyl}-9a-aza-9a-homoerythromycin

Guidance literature:: 9-deoxo-9-dihydro-9a-aza-9a-homoerithromycin A; 4-chlorosulfonylbenzene isocyanate; In toluene; at 0 - 5 ℃; for 1h;

With ammonia; In water; at 20 ℃; for 0.5h;

Reference yield:

: 690258-30-1
9-deoxo-9-dihydro-9a-N-{[4-(chlorosulfonyl)phenyl]-carbamoyl}-9a-aza-9a-homoerithromycin A

: 690258-32-3
9-deoxo-9a-{N'-[4-(aminosulfonyl)phenyl]carbamoyl}-9a-aza-9a-homoerythromycin

Guidance literature:: With ammonium hydroxide; at 20 ℃; for 2h;
DOI:10.1016/j.ejmech.2006.08.008

Reference yield:

: 6752-38-1
4-chlorosulfonylbenzene isocyanate

: 690258-32-3
9-deoxo-9a-{N'-[4-(aminosulfonyl)phenyl]carbamoyl}-9a-aza-9a-homoerythromycin

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 2 h / 0 - 5 °C

2: aq. ammonia / 2 h / 20 °C

With ammonium hydroxide; In toluene;
DOI:10.1016/j.ejmech.2006.08.008