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N-(2-Brom-5-chlorphenyl)-N-(2-bromphenyl)benzamid

Base Information
  • Chemical Name:N-(2-Brom-5-chlorphenyl)-N-(2-bromphenyl)benzamid
  • CAS No.:79370-01-7
  • Molecular Formula:C19H12Br2ClNO
  • Molecular Weight:465.571
  • Hs Code.:
N-(2-Brom-5-chlorphenyl)-N-(2-bromphenyl)benzamid

Synonyms:N-(2-Brom-5-chlorphenyl)-N-(2-bromphenyl)benzamid

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Chemical Property of N-(2-Brom-5-chlorphenyl)-N-(2-bromphenyl)benzamid
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Technology Process of N-(2-Brom-5-chlorphenyl)-N-(2-bromphenyl)benzamid

There total 5 articles about N-(2-Brom-5-chlorphenyl)-N-(2-bromphenyl)benzamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
1) 150 min, 257-260 deg C, 2) 40 deg C, 3) ethanol, 0 deg C;
DOI:10.1002/jlac.198119810715
Guidance literature:
Multi-step reaction with 4 steps
1: 93 percent / N,N-Dimethylaniline / 0.75 h / 100 °C
2: 87 percent / PCl5 / 1) 3 h, room temperature, 2) 1 h, 100 deg C
3: 78 percent / NaOEt / diethyl ether / 1) 4 h, 0 deg C, 2) 12 h, room temperature
4: 40 percent / 1) 150 min, 257-260 deg C, 2) 40 deg C, 3) ethanol, 0 deg C
With phosphorus pentachloride; sodium ethanolate; N,N-dimethyl-aniline; In diethyl ether;
DOI:10.1002/jlac.198119810715
Guidance literature:
Multi-step reaction with 5 steps
1: Raney-Ni, hydrazinhydrate
2: 93 percent / N,N-Dimethylaniline / 0.75 h / 100 °C
3: 87 percent / PCl5 / 1) 3 h, room temperature, 2) 1 h, 100 deg C
4: 78 percent / NaOEt / diethyl ether / 1) 4 h, 0 deg C, 2) 12 h, room temperature
5: 40 percent / 1) 150 min, 257-260 deg C, 2) 40 deg C, 3) ethanol, 0 deg C
With phosphorus pentachloride; sodium ethanolate; nickel; hydrazine hydrate; N,N-dimethyl-aniline; In diethyl ether;
DOI:10.1002/jlac.198119810715
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