2-bromo-N-(2-bromophenyl)-5-chloroaniline

Base Information

Chemical Name:2-bromo-N-(2-bromophenyl)-5-chloroaniline
CAS No.:79370-02-8
Molecular Formula:C₁₂H₈Br₂ClN
Molecular Weight:361.463
Hs Code.:

Synonyms:2-bromo-N-(2-bromophenyl)-5-chloroaniline

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Chemical Property of 2-bromo-N-(2-bromophenyl)-5-chloroaniline

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Technology Process of 2-bromo-N-(2-bromophenyl)-5-chloroaniline

There total 7 articles about 2-bromo-N-(2-bromophenyl)-5-chloroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 583-55-1
1-Bromo-2-iodobenzene

: 823-57-4
2-bromo-5-chloroaniline

: 79370-02-8
2-bromo-N-(2-bromophenyl)-5-chloroaniline

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate; In toluene; at 120 ℃; for 24h;
DOI:10.1021/acs.orglett.1c00573

Reference yield: 86.0%

: 79370-01-7
N-(2-Brom-5-chlorphenyl)-N-(2-bromphenyl)benzamid

: 79370-02-8
2-bromo-N-(2-bromophenyl)-5-chloroaniline

Guidance literature:: With potassium hydroxide; In ethanol; water; for 40h; Heating;
DOI:10.1002/jlac.198119810715

Reference yield:

: 823-57-4
2-bromo-5-chloroaniline

: 79370-02-8
2-bromo-N-(2-bromophenyl)-5-chloroaniline

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / N,N-Dimethylaniline / 0.75 h / 100 °C

2: 87 percent / PCl₅ / 1) 3 h, room temperature, 2) 1 h, 100 deg C

3: 78 percent / NaOEt / diethyl ether / 1) 4 h, 0 deg C, 2) 12 h, room temperature

4: 40 percent / 1) 150 min, 257-260 deg C, 2) 40 deg C, 3) ethanol, 0 deg C

5: 86 percent / KOH / ethanol; H₂O / 40 h / Heating

With potassium hydroxide; phosphorus pentachloride; sodium ethanolate; N,N-dimethyl-aniline; In diethyl ether; ethanol; water;
DOI:10.1002/jlac.198119810715