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Technology Process of (PCH3(C6H5)2)2Pt(CH3)((CH3)3PCH2C6H4NC)(2+)*2BF4(1-)*0.5CH2Cl2=[(PCH3(C6H5)2)2Pt(CH3)((CH3)3PCH2C6H4NCBF4)]BF4*0.5CH2Cl2

(PCH3(C6H5)2)2Pt(CH3)((CH3)3PCH2C6H4NC)(2+)*2BF4(1-)*0.5CH2Cl2=[(PCH3(C6H5)2)2Pt(CH3)((CH3)3PCH2C6H4NCBF4)]BF4*0.5CH2Cl2

Base Information
  • Chemical Name:(PCH3(C6H5)2)2Pt(CH3)((CH3)3PCH2C6H4NC)(2+)*2BF4(1-)*0.5CH2Cl2=[(PCH3(C6H5)2)2Pt(CH3)((CH3)3PCH2C6H4NCBF4)]BF4*0.5CH2Cl2
  • CAS No.:104241-72-7
  • Molecular Formula:2BF4*0CH2Cl2*C38H44NP3Pt
  • Molecular Weight:1018.85
  • Hs Code.:
(PCH<sub>3</sub>(C<sub>6</sub>H<sub>5</sub>)2)2Pt(CH<sub>3</sub>)((CH<sub>3</sub>)3PCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>NC)<sup>(2+)</sup>*2BF<sub>4</sub><sup>(1-)</sup>*0.5CH<sub>2</sub>Cl<sub>2</sub>=[(PCH<sub>3</sub>(C<sub>6</sub>H<sub>5</sub>)2)2Pt(CH<sub>3</sub>)((CH<sub>3</sub>)3PCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>NCBF<sub>4</sub>)]BF<sub>4</sub>*0.5CH<sub>2</sub>Cl<sub>2</sub>

Synonyms:(PCH3(C6H5)2)2Pt(CH3)((CH3)3PCH2C6H4NC)(2+)*2BF4(1-)*0.5CH2Cl2=[(PCH3(C6H5)2)2Pt(CH3)((CH3)3PCH2C6H4NCBF4)]BF4*0.5CH2Cl2

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Chemical Property of (PCH3(C6H5)2)2Pt(CH3)((CH3)3PCH2C6H4NC)(2+)*2BF4(1-)*0.5CH2Cl2=[(PCH3(C6H5)2)2Pt(CH3)((CH3)3PCH2C6H4NCBF4)]BF4*0.5CH2Cl2
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Technology Process of (PCH3(C6H5)2)2Pt(CH3)((CH3)3PCH2C6H4NC)(2+)*2BF4(1-)*0.5CH2Cl2=[(PCH3(C6H5)2)2Pt(CH3)((CH3)3PCH2C6H4NCBF4)]BF4*0.5CH2Cl2

There total 1 articles about (PCH3(C6H5)2)2Pt(CH3)((CH3)3PCH2C6H4NC)(2+)*2BF4(1-)*0.5CH2Cl2=[(PCH3(C6H5)2)2Pt(CH3)((CH3)3PCH2C6H4NCBF4)]BF4*0.5CH2Cl2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

silver tetrafluoroborate
14104-20-2

silver tetrafluoroborate

trans-[PtMeCl(PMePh<sub>2</sub>)2]
24833-61-2

trans-[PtMeCl(PMePh2)2]

(CH<sub>3</sub>)3PCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>NC<sup>(1+)</sup>*BF<sub>4</sub><sup>(1-)</sup>={(CH<sub>3</sub>)3PCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>NC}{BF<sub>4</sub>}
104292-21-9

(CH3)3PCH2C6H4NC(1+)*BF4(1-)={(CH3)3PCH2C6H4NC}{BF4}

(PCH<sub>3</sub>(C<sub>6</sub>H<sub>5</sub>)2)2Pt(CH<sub>3</sub>)((CH<sub>3</sub>)3PCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>NC)<sup>(2+)</sup>*2BF<sub>4</sub><sup>(1-)</sup>*0.5CH<sub>2</sub>Cl<sub>2</sub>=[(PCH<sub>3</sub>(C<sub>6</sub>H<sub>5</sub>)2)2Pt(CH<sub>3</sub>)((CH<sub>3</sub>)3PCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>NCBF<sub>4</sub>)]BF<sub>4</sub>*0.5CH<sub>2</sub>Cl<sub>2</sub>
104241-72-7

(PCH3(C6H5)2)2Pt(CH3)((CH3)3PCH2C6H4NC)(2+)*2BF4(1-)*0.5CH2Cl2=[(PCH3(C6H5)2)2Pt(CH3)((CH3)3PCH2C6H4NCBF4)]BF4*0.5CH2Cl2

Guidance literature:
In dichloromethane; acetone; byproducts: AgCl; N2-atmosphere; addn. of AgBF4 (1 equiv.) to Pt-complex in acetone (0°C), stirring (30 min, room temp.), filtration, addn. of isonitrile (in CH2Cl2, 0°C), stirring (2 h); concn., Et2O addn.; elem. anal.;

Reference yield: 68.0%

(PCH<sub>3</sub>(C<sub>6</sub>H<sub>5</sub>)2)2Pt(CH<sub>3</sub>)((CH<sub>3</sub>)3PCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>NC)<sup>(2+)</sup>*2BF<sub>4</sub><sup>(1-)</sup>*0.5CH<sub>2</sub>Cl<sub>2</sub>=[(PCH<sub>3</sub>(C<sub>6</sub>H<sub>5</sub>)2)2Pt(CH<sub>3</sub>)((CH<sub>3</sub>)3PCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>NCBF<sub>4</sub>)]BF<sub>4</sub>*0.5CH<sub>2</sub>Cl<sub>2</sub>
104241-72-7

(PCH3(C6H5)2)2Pt(CH3)((CH3)3PCH2C6H4NC)(2+)*2BF4(1-)*0.5CH2Cl2=[(PCH3(C6H5)2)2Pt(CH3)((CH3)3PCH2C6H4NCBF4)]BF4*0.5CH2Cl2

(PCH<sub>3</sub>(C<sub>6</sub>H<sub>5</sub>)2)2Pt(CN(H)C<sub>6</sub>H<sub>4</sub>C(P(CH<sub>3</sub>)3))Cl<sup>(1+)</sup>*BF<sub>4</sub><sup>(1-)</sup>*0.5CH<sub>2</sub>Cl<sub>2</sub>=[(PCH<sub>3</sub>(C<sub>6</sub>H<sub>5</sub>)2)2Pt(CN(H)C<sub>6</sub>H<sub>4</sub>C(P(CH<sub>3</sub>)3))Cl]BF<sub>4</sub>*0.5CH<sub>2</sub>Cl<sub>2</sub>
104241-80-7

(PCH3(C6H5)2)2Pt(CN(H)C6H4C(P(CH3)3))Cl(1+)*BF4(1-)*0.5CH2Cl2=[(PCH3(C6H5)2)2Pt(CN(H)C6H4C(P(CH3)3))Cl]BF4*0.5CH2Cl2

Guidance literature:
With NEt3; In dichloromethane; byproducts: [HNEt3]BF4; N2-atmosphere; stirring (room temp., 2 days); concn., pptn. on Et2O addn., filtration, drying (vac.); elem. anal.;
upstream raw materials:

silver tetrafluoroborate

trans-[PtMeCl(PMePh2)2]

(CH3)3PCH2C6H4NC(1+)*BF4(1-)={(CH3)3PCH2C6H4NC}{BF4}

Downstream raw materials:

(PCH3(C6H5)2)2Pt(CN(H)C6H4C(P(CH3)3))Cl(1+)*BF4(1-)*0.5CH2Cl2=[(PCH3(C6H5)2)2Pt(CN(H)C6H4C(P(CH3)3))Cl]BF4*0.5CH2Cl2

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