6-(2-phenylethoxy)pyridine-3-boronic acid

Base Information

Chemical Name:6-(2-phenylethoxy)pyridine-3-boronic acid
CAS No.:1270921-82-8
Molecular Formula:C₁₃H₁₄BNO₃
Molecular Weight:243.07
Hs Code.:

Synonyms:6-(2-phenylethoxy)pyridine-3-boronic acid

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Chemical Property of 6-(2-phenylethoxy)pyridine-3-boronic acid

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Technology Process of 6-(2-phenylethoxy)pyridine-3-boronic acid

There total 4 articles about 6-(2-phenylethoxy)pyridine-3-boronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₂₆BNO₃

: 1270921-82-8
6-(2-phenylethoxy)pyridine-3-boronic acid

Guidance literature:: C₁₉H₂₆BNO₃; With sodium hydroxide; In water; at 20 ℃;

With hydrogenchloride; In water;
DOI:10.1016/j.ejmech.2015.02.056

Reference yield:

: 60-12-8
2-phenylethanol

: 1270921-82-8
6-(2-phenylethoxy)pyridine-3-boronic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran / 1.5 h / 0 - 20 °C / Reflux

1.2: 12 h / Reflux

2.1: n-butyllithium / diethyl ether; tetrahydrofuran / 1 h / -78 °C

2.2: 1 h

3.1: sodium hydroxide / water / 20 °C

With n-butyllithium; sodium hydride; sodium hydroxide; In tetrahydrofuran; diethyl ether; water;
DOI:10.1016/j.ejmech.2015.02.056

Reference yield:

: 766-11-0
5-bromo-2-fluoropyridine

: 1270921-82-8
6-(2-phenylethoxy)pyridine-3-boronic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran / 1.5 h / 0 - 20 °C / Reflux

1.2: 12 h / Reflux

2.1: n-butyllithium / diethyl ether; tetrahydrofuran / 1 h / -78 °C

2.2: 1 h

3.1: sodium hydroxide / water / 20 °C

With n-butyllithium; sodium hydride; sodium hydroxide; In tetrahydrofuran; diethyl ether; water;
DOI:10.1016/j.ejmech.2015.02.056