[(2,6-diisopropylphenyl)N=CMe-CMe=N(2,6-diisopropylphenyl)]Pd[CH₂CHMeCH(OMe)2]B[3,5-(CF₃)2C₆H₃]4

Base Information

• Chemical Name: [(2,6-diisopropylphenyl)N=CMe-CMe=N(2,6-diisopropylphenyl)]Pd[CH₂CHMeCH(OMe)2]B[3,5-(CF₃)2C₆H₃]4
• CAS No.: 791114-71-1
• Molecular Formula: C₃₂H₁₂BF₂₄*C₃₄H₅₃N₂O₂Pd
• Molecular Weight: 1491.45

Synonyms:[(2,6-diisopropylphenyl)N=CMe-CMe=N(2,6-diisopropylphenyl)]Pd[CH₂CHMeCH(OMe)2]B[3,5-(CF₃)2C₆H₃]4

Chemical Property of [(2,6-diisopropylphenyl)N=CMe-CMe=N(2,6-diisopropylphenyl)]Pd[CH₂CHMeCH(OMe)2]B[3,5-(CF₃)2C₆H₃]4

Chemical Property:

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Technology Process of [(2,6-diisopropylphenyl)N=CMe-CMe=N(2,6-diisopropylphenyl)]Pd[CH₂CHMeCH(OMe)2]B[3,5-(CF₃)2C₆H₃]4

There total 1 articles about [(2,6-diisopropylphenyl)N=CMe-CMe=N(2,6-diisopropylphenyl)]Pd[CH₂CHMeCH(OMe)2]B[3,5-(CF₃)2C₆H₃]4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,3-dimethoxyprop-1-ene (6044-68-4) + [(2,6-iPrC6H3NC(Me)C(Me)N-2,6-iPrC6H3)Pd(CH3)(Cl)] + sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate (79060-88-1) → [(2,6-diisopropylphenyl)N=CMe-CMe=N(2,6-diisopropylphenyl)]Pd[CH2CHMeCH(OMe)2]B[3,5-(CF3)2C6H3]4 (791114-71-1)

Guidance literature:

In dichloromethane; identified by (1) and (13)C NMR spectroscopy, elem. anal., and single-crystal X-ray structure detn.;

DOI:10.1021/ja045948y

Reference yield: 80.0%

3,3-dimethoxyprop-1-ene (6044-68-4) + [(2,6-diisopropylphenyl)N=CMe-CMe=N(2,6-diisopropylphenyl)]Pd[CH2CHMeCH(OMe)2]B[3,5-(CF3)2C6H3]4 (791114-71-1) → [(2,6-diisopropylphenyl)N=CMe-CMe=N(2,6-diisopropylphenyl)]Pd(η3-1-MeOCHCHCH2)B[3,5-(CF3)2C6H3]4 (791114-73-3)

Guidance literature:

With ethene; In dichloromethane; byproducts: ethene/acrolein dimethyl acetal copolymer; room temp., 20 h; identified by NMR spectroscopy, elem. anal., and single-crystal X-ray structure detn.;

DOI:10.1021/ja045948y

Reference yield:

3-ethoxyprop-1-ene (557-31-3) + [(2,6-diisopropylphenyl)N=CMe-CMe=N(2,6-diisopropylphenyl)]Pd[CH2CHMeCH(OMe)2]B[3,5-(CF3)2C6H3]4 (791114-71-1) → [(2,6-diisopropylphenyl)N=CMe-CMe=N(2,6-diisopropylphenyl)]Pd(η3-CH2CHCH2)B[3,5-(CF3)2C6H3]4 (791114-75-5)

Guidance literature:

With ethene; In not given; byproducts: ethanol; excess of AllOEt; Pd-complex was identified by NMR spectroscopy, formation of EtOH was observed by GC/MS anal.;

DOI:10.1021/ja045948y

upstream raw materials:

3,3-dimethoxyprop-1-ene

sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

Downstream raw materials:

[(2,6-diisopropylphenyl)N=CMe-CMe=N(2,6-diisopropylphenyl)]Pd(η3-1-MeOCHCHCH2)B[3,5-(CF3)2C6H3]4

[(2,6-diisopropylphenyl)N=CMe-CMe=N(2,6-diisopropylphenyl)]Pd(η3-CH2CHCH2)B[3,5-(CF3)2C6H3]4

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