(E)-N,N-dimethyl-N-(2-(4-nitrophenoxy)-2-oxoethyl)-3-phenylprop-2-en-1-aminium bromide

Base Information

Chemical Name:(E)-N,N-dimethyl-N-(2-(4-nitrophenoxy)-2-oxoethyl)-3-phenylprop-2-en-1-aminium bromide
CAS No.:1581720-05-9
Molecular Formula:Br*C₁₉H₂₁N₂O₄
Molecular Weight:421.291
Hs Code.:

Synonyms:(E)-N,N-dimethyl-N-(2-(4-nitrophenoxy)-2-oxoethyl)-3-phenylprop-2-en-1-aminium bromide

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Chemical Property of (E)-N,N-dimethyl-N-(2-(4-nitrophenoxy)-2-oxoethyl)-3-phenylprop-2-en-1-aminium bromide

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Technology Process of (E)-N,N-dimethyl-N-(2-(4-nitrophenoxy)-2-oxoethyl)-3-phenylprop-2-en-1-aminium bromide

There total 6 articles about (E)-N,N-dimethyl-N-(2-(4-nitrophenoxy)-2-oxoethyl)-3-phenylprop-2-en-1-aminium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 1581720-05-9
(E)-N,N-dimethyl-N-(2-(4-nitrophenoxy)-2-oxoethyl)-3-phenylprop-2-en-1-aminium bromide

Guidance literature:: Multi-step reaction with 5 steps

1: dichloromethane / 20 - 25 °C / Inert atmosphere

2: diisobutylaluminium hydride / dichloromethane; toluene / 1.5 h / -78 °C / Inert atmosphere

3: phosphorus tribromide / diethyl ether / 0 °C / Inert atmosphere; Darkness

4: tetrahydrofuran; water / 0.17 h / 20 - 25 °C / Inert atmosphere

5: acetonitrile / 1 h / 20 - 25 °C / Inert atmosphere

With phosphorus tribromide; diisobutylaluminium hydride; In tetrahydrofuran; diethyl ether; dichloromethane; water; toluene; acetonitrile;
DOI:10.1021/ja500758n

Reference yield:

: 24393-61-1
ethyl (E)-3-(4-nitrophenyl)-2-propenoate

: 1581720-05-9
(E)-N,N-dimethyl-N-(2-(4-nitrophenoxy)-2-oxoethyl)-3-phenylprop-2-en-1-aminium bromide

Guidance literature:: Multi-step reaction with 4 steps

1: diisobutylaluminium hydride / dichloromethane; toluene / 1.5 h / -78 °C / Inert atmosphere

2: phosphorus tribromide / diethyl ether / 0 °C / Inert atmosphere; Darkness

3: tetrahydrofuran; water / 0.17 h / 20 - 25 °C / Inert atmosphere

4: acetonitrile / 1 h / 20 - 25 °C / Inert atmosphere

With phosphorus tribromide; diisobutylaluminium hydride; In tetrahydrofuran; diethyl ether; dichloromethane; water; toluene; acetonitrile;
DOI:10.1021/ja500758n

Reference yield:

: 35271-56-8
(E)-4-nitrocinnamyl alcohol

: 1581720-05-9
(E)-N,N-dimethyl-N-(2-(4-nitrophenoxy)-2-oxoethyl)-3-phenylprop-2-en-1-aminium bromide

Guidance literature:: Multi-step reaction with 3 steps

1: phosphorus tribromide / diethyl ether / 0 °C / Inert atmosphere; Darkness

2: tetrahydrofuran; water / 0.17 h / 20 - 25 °C / Inert atmosphere

3: acetonitrile / 1 h / 20 - 25 °C / Inert atmosphere

With phosphorus tribromide; In tetrahydrofuran; diethyl ether; water; acetonitrile;
DOI:10.1021/ja500758n