N-methyl-N'-methyl-N'-{3-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}acetohydrazide

Base Information

Chemical Name:N-methyl-N'-methyl-N'-{3-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}acetohydrazide
CAS No.:1237587-19-7
Molecular Formula:C₂₀H₁₈Cl₂F₃N₃O₂
Molecular Weight:460.283
Hs Code.:

Synonyms:N-methyl-N'-methyl-N'-{3-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}acetohydrazide

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Chemical Property of N-methyl-N'-methyl-N'-{3-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}acetohydrazide

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Technology Process of N-methyl-N'-methyl-N'-{3-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}acetohydrazide

There total 10 articles about N-methyl-N'-methyl-N'-{3-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}acetohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1237587-18-6
N'-methyl-N'-{3-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]phenyl}acetohydrazide

: 74-88-4
methyl iodide

: 1237587-19-7
N-methyl-N'-methyl-N'-{3-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}acetohydrazide

Guidance literature:: With sodium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 5h;

Reference yield:

: 3431-62-7,20747-39-1
3-nitrobenzaldoxime

: 1237587-19-7
N-methyl-N'-methyl-N'-{3-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}acetohydrazide

Guidance literature:: Multi-step reaction with 9 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 60 °C

1.2: 6 h / 20 °C

2.1: acetic acid; iron / ethanol; water / 1.25 h / 20 - 75 °C

3.1: triethylamine / tetrahydrofuran / 0.25 h / 0 °C

4.1: sodium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C

5.1: water; sodium carbonate / methanol / 2 h / 20 °C

6.1: hydrogenchloride / water; tetrahydrofuran / 0.25 h / 20 °C

6.2: 1 h / 0 °C

7.1: zinc; acetic acid / ethanol; water / 5 h / 20 °C

8.1: triethylamine / tetrahydrofuran / 1 h / 0 °C

9.1: sodium carbonate / N,N-dimethyl-formamide / 5 h / 20 °C

With hydrogenchloride; N-chloro-succinimide; water; iron; sodium carbonate; acetic acid; triethylamine; zinc; In tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: 1070396-55-2
3-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]nitrobenzene

: 1237587-19-7
N-methyl-N'-methyl-N'-{3-[5-(3,5-dichlorophenyl)-5-trifluoro methyl-4,5-dihydroisoxazol-3-yl]phenyl}acetohydrazide

Guidance literature:: Multi-step reaction with 8 steps

1.1: acetic acid; iron / ethanol; water / 1.25 h / 20 - 75 °C

2.1: triethylamine / tetrahydrofuran / 0.25 h / 0 °C

3.1: sodium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C

4.1: water; sodium carbonate / methanol / 2 h / 20 °C

5.1: hydrogenchloride / water; tetrahydrofuran / 0.25 h / 20 °C

5.2: 1 h / 0 °C

6.1: zinc; acetic acid / ethanol; water / 5 h / 20 °C

7.1: triethylamine / tetrahydrofuran / 1 h / 0 °C

8.1: sodium carbonate / N,N-dimethyl-formamide / 5 h / 20 °C

With hydrogenchloride; water; iron; sodium carbonate; acetic acid; triethylamine; zinc; In tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide;