2-hydroxy-1-(4-nitro) acetophenone thiosemicarbazone hemisuccinate ester

Base Information

Chemical Name:2-hydroxy-1-(4-nitro) acetophenone thiosemicarbazone hemisuccinate ester
CAS No.:1456532-33-4
Molecular Formula:C₁₃H₁₄N₄O₆S
Molecular Weight:354.343
Hs Code.:

Synonyms:2-hydroxy-1-(4-nitro) acetophenone thiosemicarbazone hemisuccinate ester

Suppliers and Price of 2-hydroxy-1-(4-nitro) acetophenone thiosemicarbazone hemisuccinate ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-hydroxy-1-(4-nitro) acetophenone thiosemicarbazone hemisuccinate ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-hydroxy-1-(4-nitro) acetophenone thiosemicarbazone hemisuccinate ester

There total 3 articles about 2-hydroxy-1-(4-nitro) acetophenone thiosemicarbazone hemisuccinate ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-30-5
succinic acid anhydride

: 1456532-31-2
2-hydroxy-1-(4-nitro)acetophenone thiosemicarbazone

: 1456532-33-4
2-hydroxy-1-(4-nitro) acetophenone thiosemicarbazone hemisuccinate ester

Guidance literature:: With dmap; In acetonitrile; at 20 ℃; for 48h;
DOI:10.1016/j.ejmech.2013.04.022

Reference yield:

: 99-81-0
4-Nitrophenacyl bromide

: 1456532-33-4
2-hydroxy-1-(4-nitro) acetophenone thiosemicarbazone hemisuccinate ester

Guidance literature:: Multi-step reaction with 3 steps

1: silver nitrate / water; acetone / 4 h / Reflux

2: acetic acid / ethanol / 24 h / 20 °C

3: dmap / acetonitrile / 48 h / 20 °C

With dmap; silver nitrate; acetic acid; In ethanol; water; acetone; acetonitrile;
DOI:10.1016/j.ejmech.2013.04.022

Reference yield:

: 64611-67-2
2-hydroxy-1-(4-nitrophenyl)ethanone

: 1456532-33-4
2-hydroxy-1-(4-nitro) acetophenone thiosemicarbazone hemisuccinate ester

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / ethanol / 24 h / 20 °C

2: dmap / acetonitrile / 48 h / 20 °C

With dmap; acetic acid; In ethanol; acetonitrile;
DOI:10.1016/j.ejmech.2013.04.022