C₄₇H₅₆N₆O₁₀

Base Information

Chemical Name:C₄₇H₅₆N₆O₁₀
CAS No.:675129-57-4
Molecular Formula:C₄₇H₅₆N₆O₁₀
Molecular Weight:864.996
Hs Code.:

C<sub>47</sub>H<sub>56</sub>N<sub>6</sub>O<sub>10</sub>

Synonyms:C₄₇H₅₆N₆O₁₀

Suppliers and Price of C₄₇H₅₆N₆O₁₀

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₇H₅₆N₆O₁₀

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₇H₅₆N₆O₁₀

There total 13 articles about C₄₇H₅₆N₆O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 675129-54-1
C₅₂H₆₄N₆O₁₂

: 675129-57-4
C₄₇H₅₆N₆O₁₀

Guidance literature:: With trifluoroacetic acid; at 20 ℃; for 0.5h;
DOI:10.1021/jo030293p

Reference yield:

: 86099-14-1
(2S)-3-(4-hydroxyphenyl)-2-(methyl{[(phenylmethyl)oxy]carbonyl}amino)propanoic acid

: 675129-57-4
C₄₇H₅₆N₆O₁₀

Guidance literature:: Multi-step reaction with 9 steps

1: 71 percent / HOBt; Et₃N; EDC / CH₂Cl₂ / 16 h / 20 °C

2: 100 percent / methanol; diethyl ether

3: H₂; hydrochloric acid / Pd/C / methanol / 2 h / 20 °C

4: 587 mg / PyBOP; iPr₂NEt / CH₂Cl₂ / 120 h / -20 - 20 °C

5: TFA / 2 h / 20 °C

6: 376 mg / HOBt; EDC / CH₂Cl₂ / 25 h / -20 - 20 °C

7: 99 percent / LiOH*H₂O / tetrahydrofuran; methanol; H₂O / 3 h / 20 °C

8: 38.4 mg / 3-hydroxy-4-oxo-3,4-dihydro-1,2,3-benzotriazine; EDC / tetrahydrofuran / 48 h / 20 °C

9: 95 percent / TFA / 0.5 h / 20 °C

With hydrogenchloride; lithium hydroxide; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; N-ethyl-N,N-diisopropylamine; 3-hydroxy-3,4-dihydrobenzotriazine-4-one; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water;
DOI:10.1021/jo030293p

Reference yield:

: 115441-64-0
methyl N-Cbz-N-methyl-L-tyrosyl-L-alaninate

: 675129-57-4
C₄₇H₅₆N₆O₁₀

Guidance literature:: Multi-step reaction with 8 steps

1: 100 percent / methanol; diethyl ether

2: H₂; hydrochloric acid / Pd/C / methanol / 2 h / 20 °C

3: 587 mg / PyBOP; iPr₂NEt / CH₂Cl₂ / 120 h / -20 - 20 °C

4: TFA / 2 h / 20 °C

5: 376 mg / HOBt; EDC / CH₂Cl₂ / 25 h / -20 - 20 °C

6: 99 percent / LiOH*H₂O / tetrahydrofuran; methanol; H₂O / 3 h / 20 °C

7: 38.4 mg / 3-hydroxy-4-oxo-3,4-dihydro-1,2,3-benzotriazine; EDC / tetrahydrofuran / 48 h / 20 °C

8: 95 percent / TFA / 0.5 h / 20 °C

With hydrogenchloride; lithium hydroxide; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; 3-hydroxy-3,4-dihydrobenzotriazine-4-one; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water;
DOI:10.1021/jo030293p