((2S,3R,E)-4,4-difluoro-3-vunyloct-6-ene-1,2,5-triyl)tris(oxy)tris(methylene)tribenzene

Base Information

Chemical Name:((2S,3R,E)-4,4-difluoro-3-vunyloct-6-ene-1,2,5-triyl)tris(oxy)tris(methylene)tribenzene
CAS No.:1159099-69-0
Molecular Formula:C₃₁H₃₄F₂O₃
Molecular Weight:492.606
Hs Code.:

Synonyms:((2S,3R,E)-4,4-difluoro-3-vunyloct-6-ene-1,2,5-triyl)tris(oxy)tris(methylene)tribenzene

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Chemical Property of ((2S,3R,E)-4,4-difluoro-3-vunyloct-6-ene-1,2,5-triyl)tris(oxy)tris(methylene)tribenzene

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Technology Process of ((2S,3R,E)-4,4-difluoro-3-vunyloct-6-ene-1,2,5-triyl)tris(oxy)tris(methylene)tribenzene

There total 1 articles about ((2S,3R,E)-4,4-difluoro-3-vunyloct-6-ene-1,2,5-triyl)tris(oxy)tris(methylene)tribenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1001273-22-8
(R,E)-6-((S)-1,2-bis(benzyloxy)ethyl)-5,5-difluoroocta-2,7-dien-4-ol

: 100-39-0
benzyl bromide

: 1159099-69-0
((2S,3R,E)-4,4-difluoro-3-vunyloct-6-ene-1,2,5-triyl)tris(oxy)tris(methylene)tribenzene

Guidance literature:: (R,E)-6-((S)-1,2-bis(benzyloxy)ethyl)-5,5-difluoroocta-2,7-dien-4-ol; With tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; Inert atmosphere;

benzyl bromide; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2009.02.079

Reference yield: 43.0%

: 1159099-69-0
((2S,3R,E)-4,4-difluoro-3-vunyloct-6-ene-1,2,5-triyl)tris(oxy)tris(methylene)tribenzene

: 1159099-71-4
(2S,4R)-2-(benzyloxy)-4-((S)-1,2-bis(benzyloxy)ethyl)-3,3-difluoropentane-1,5-diol

: 1159099-70-3
(2R,4R)-2-(benzyloxy)-4-((S)-1,2-bis(benzyloxy)ethyl)-3,3-difluoropentane-1,5-diol

Guidance literature:: ((2S,3R,E)-4,4-difluoro-3-vunyloct-6-ene-1,2,5-triyl)tris(oxy)tris(methylene)tribenzene; With ozone; In methanol; dichloromethane; at -78 ℃;

With sodium tetrahydroborate; In methanol; dichloromethane; for 1h;

With water; ammonium chloride; In methanol; dichloromethane;
DOI:10.1016/j.tet.2009.02.079