(R,E)-6-(benzyloxy)-1-(methoxymethoxy)hex-3-en-2-yl 2-(2-methoxyphenyl)acetate

Base Information

Chemical Name:(R,E)-6-(benzyloxy)-1-(methoxymethoxy)hex-3-en-2-yl 2-(2-methoxyphenyl)acetate
CAS No.:1630067-73-0
Molecular Formula:C₂₄H₃₀O₆
Molecular Weight:414.499
Hs Code.:

Synonyms:(R,E)-6-(benzyloxy)-1-(methoxymethoxy)hex-3-en-2-yl 2-(2-methoxyphenyl)acetate

Suppliers and Price of (R,E)-6-(benzyloxy)-1-(methoxymethoxy)hex-3-en-2-yl 2-(2-methoxyphenyl)acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R,E)-6-(benzyloxy)-1-(methoxymethoxy)hex-3-en-2-yl 2-(2-methoxyphenyl)acetate

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Technology Process of (R,E)-6-(benzyloxy)-1-(methoxymethoxy)hex-3-en-2-yl 2-(2-methoxyphenyl)acetate

There total 1 articles about (R,E)-6-(benzyloxy)-1-(methoxymethoxy)hex-3-en-2-yl 2-(2-methoxyphenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.1%

: 93-25-4
2-methoxyphenylacetic acid

: 1630067-58-1
(R,E)-6-(benzyloxy)-1-(methoxymethoxy)hex-3-en-2-ol

: 1630067-73-0
(R,E)-6-(benzyloxy)-1-(methoxymethoxy)hex-3-en-2-yl 2-(2-methoxyphenyl)acetate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃; for 3h; Inert atmosphere;
DOI:10.1002/ejoc.201402452

Reference yield: 86.3%

: 1630067-73-0
(R,E)-6-(benzyloxy)-1-(methoxymethoxy)hex-3-en-2-yl 2-(2-methoxyphenyl)acetate

: 1630067-74-1
(2S,3R,E)-3-[2-(benzyloxy)ethyl]-6-(methoxymethoxy)-2-(2-methoxyphenyl)hex-4-enoic acid

Guidance literature:: With chloro-trimethyl-silane; lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; at -78 - -20 ℃; for 2.75h; Inert atmosphere;
DOI:10.1002/ejoc.201402452

Reference yield:

: 1630067-73-0
(R,E)-6-(benzyloxy)-1-(methoxymethoxy)hex-3-en-2-yl 2-(2-methoxyphenyl)acetate

: 1630067-75-2
(2S,3R,E)-3-[2-(benzyloxy)ethyl]-6-(methoxymethoxy)-2-(2-methoxyphenyl)hex-4-enamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: chloro-trimethyl-silane; lithium hexamethyldisilazane / tetrahydrofuran; diethyl ether / 2.75 h / -78 - -20 °C / Inert atmosphere

2.1: di-tert-butyl dicarbonate; pyridine / ethyl acetate / 3.5 h / 20 °C / Inert atmosphere

2.2: 1 h / Inert atmosphere

With pyridine; chloro-trimethyl-silane; di-tert-butyl dicarbonate; lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; ethyl acetate;
DOI:10.1002/ejoc.201402452