Technology Process of C28H25FN4O4S2
There total 4 articles about C28H25FN4O4S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
4-(4-bromothiazol-2-yl)morpholine; C27H28BFN2O5S;
With
caesium carbonate;
In
acetonitrile;
for 0.166667h;
Inert atmosphere;
With
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2;
In
N,N-dimethyl-formamide;
at 80 ℃;
Inert atmosphere;
Sealed tube;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: caesium carbonate / acetonitrile / 0.25 h / Inert atmosphere; Sealed tube
1.2: 6.25 h / 90 °C / Inert atmosphere
2.1: potassium acetate / N,N-dimethyl-formamide / 0.17 h / Inert atmosphere
2.2: 2.17 h / 100 °C / Inert atmosphere
3.1: caesium carbonate / acetonitrile / 0.17 h / Inert atmosphere
3.2: 80 °C / Inert atmosphere; Sealed tube
With
potassium acetate; caesium carbonate;
In
N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: caesium carbonate / acetonitrile / 0.25 h / Inert atmosphere; Sealed tube
1.2: 6.25 h / 90 °C / Inert atmosphere
2.1: potassium acetate / N,N-dimethyl-formamide / 0.17 h / Inert atmosphere
2.2: 2.17 h / 100 °C / Inert atmosphere
3.1: caesium carbonate / acetonitrile / 0.17 h / Inert atmosphere
3.2: 80 °C / Inert atmosphere; Sealed tube
With
potassium acetate; caesium carbonate;
In
N,N-dimethyl-formamide; acetonitrile;