[2,6-(2,4,6-Me3C6H2)2C6H3N=][2-(η5-2,4,6-Me3C6H3)-6-(2,4,6-Me3C6H2)C6H3NH]Ta(OSO2CF3)

Base Information

Chemical Name:[2,6-(2,4,6-Me3C6H2)2C6H3N=][2-(η5-2,4,6-Me3C6H3)-6-(2,4,6-Me3C6H2)C6H3NH]Ta(OSO2CF3)
CAS No.:450374-35-3
Molecular Formula:C₄₉H₅₂F₃N₂O₃STa
Molecular Weight:986.973
Hs Code.:

Synonyms:[2,6-(2,4,6-Me3C6H2)2C6H3N=][2-(η5-2,4,6-Me3C6H3)-6-(2,4,6-Me3C6H2)C6H3NH]Ta(OSO2CF3)

Suppliers and Price of [2,6-(2,4,6-Me3C6H2)2C6H3N=][2-(η5-2,4,6-Me3C6H3)-6-(2,4,6-Me3C6H2)C6H3NH]Ta(OSO2CF3)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [2,6-(2,4,6-Me3C6H2)2C6H3N=][2-(η5-2,4,6-Me3C6H3)-6-(2,4,6-Me3C6H2)C6H3NH]Ta(OSO2CF3)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [2,6-(2,4,6-Me3C6H2)2C6H3N=][2-(η5-2,4,6-Me3C6H3)-6-(2,4,6-Me3C6H2)C6H3NH]Ta(OSO2CF3)

There total 7 articles about [2,6-(2,4,6-Me3C6H2)2C6H3N=][2-(η5-2,4,6-Me3C6H3)-6-(2,4,6-Me3C6H2)C6H3NH]Ta(OSO2CF3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: (2,6-(2,4,6-Me₃C₆H₂)2C₆H₃N=)(2,6-(2,4,6-Me₃C₆H₂)2C₆H₃NH)TaMe(OSO₂CF₃)*0.5(pentane)

: 1333-74-0
hydrogen

: 450374-35-3
[2,6-(2,4,6-Me3C6H2)2C6H3N=][2-(η5-2,4,6-Me3C6H3)-6-(2,4,6-Me3C6H2)C6H3NH]Ta(OSO2CF3)

Guidance literature:: With 1-hexene; In further solvent(s); byproducts: n-hexane; soln. of Ta complex in bromobenzene-d5 heated at 95°C under H2 (1atm) in presence of 1-hexene; not isolated; detd. by NMR spectra;
DOI:10.1021/om020509y

Reference yield:

: [2,6-(2',4',6'-Me₃C₆H₂)2C₆H₃N=][2,6-(2',4',6'-Me₃C₆H₂)2C₆H₃NH]TaMe(OSO₂CF₃)

: 1333-74-0
hydrogen

: 450374-35-3
[2,6-(2,4,6-Me3C6H2)2C6H3N=][2-(η5-2,4,6-Me3C6H3)-6-(2,4,6-Me3C6H2)C6H3NH]Ta(OSO2CF3)

Guidance literature:: In further solvent(s); byproducts: methane; soln. of Ta complex in bromobenzene heated at 95°C over 2 d in presence of H2 (1 atm); recrystd. from toluene at -35°C;
DOI:10.1021/ja025684k

Reference yield:

: [2,6-(2,4,6-Me3C6H2)2C6H3N=][2-(η5-2,4,6-Me3C6H2D)-6-(2,4,6-Me3C6H2)C6H3NH]Ta(OSO2CF3)

: 1333-74-0
hydrogen

: 450374-35-3
[2,6-(2,4,6-Me3C6H2)2C6H3N=][2-(η5-2,4,6-Me3C6H3)-6-(2,4,6-Me3C6H2)C6H3NH]Ta(OSO2CF3)

Guidance literature:: In further solvent(s); soln. of Ta complex in bromobenzene-d5 heated at 95°C for 24 h inpresence of H2 (1 atm);
DOI:10.1021/ja025684k