(R)-2,3-dibenzyloxypropyl 5-chloro-5-deoxy-2,3-O-isopropylidene-β-D-riboside

Base Information

Chemical Name:(R)-2,3-dibenzyloxypropyl 5-chloro-5-deoxy-2,3-O-isopropylidene-β-D-riboside
CAS No.:370860-11-0
Molecular Formula:C₂₅H₃₁ClO₆
Molecular Weight:462.971
Hs Code.:

Synonyms:(R)-2,3-dibenzyloxypropyl 5-chloro-5-deoxy-2,3-O-isopropylidene-β-D-riboside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-2,3-dibenzyloxypropyl 5-chloro-5-deoxy-2,3-O-isopropylidene-β-D-riboside

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Technology Process of (R)-2,3-dibenzyloxypropyl 5-chloro-5-deoxy-2,3-O-isopropylidene-β-D-riboside

There total 2 articles about (R)-2,3-dibenzyloxypropyl 5-chloro-5-deoxy-2,3-O-isopropylidene-β-D-riboside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 38838-07-2
1-O-methyl-2,3-O-isopropylidene-5-chloro-5-deoxy-β-D-ribofuranoside

: 20196-71-8
(2S)-2,3-bis(benzyloxy)propanol

: 370860-11-0
(R)-2,3-dibenzyloxypropyl 5-chloro-5-deoxy-2,3-O-isopropylidene-β-D-riboside

Guidance literature:: With camphor-10-sulfonic acid; at 80 ℃; for 20h; under 25 Torr;
DOI:10.1071/CH01036

Reference yield:

: 4137-56-8
methyl 2,3-O-isopropylidene-5-O-p-tolylsulfonyl-β-D-ribofuranoside

: 370860-11-0
(R)-2,3-dibenzyloxypropyl 5-chloro-5-deoxy-2,3-O-isopropylidene-β-D-riboside

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / Bu₄NCl / dimethylformamide / 36 h / Heating

2: 40 percent / camphorsulfonic acid / 20 h / 80 °C / 25 Torr

With camphor-10-sulfonic acid; tetrabutyl-ammonium chloride; In N,N-dimethyl-formamide;
DOI:10.1071/CH01036