C₂₈H₃₁N₅O₂

Base Information

• Chemical Name: C₂₈H₃₁N₅O₂
• CAS No.: 1001014-11-4
• Molecular Formula: C₂₈H₃₁N₅O₂
• Molecular Weight: 469.586
• Mol file: 1001014-11-4.mol

Synonyms:C₂₈H₃₁N₅O₂

Chemical Property of C₂₈H₃₁N₅O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₂₈H₃₁N₅O₂

There total 6 articles about C₂₈H₃₁N₅O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[2-(4-amino-phenyl)-ethyl]-methyl-carbamic acid tert-butyl ester (144222-24-2) + 4-(1H-pyrrolo[2,3-b]pyridin-1-yl)benzonitrile (1001013-59-7) → C28H31N5O2 (1001014-11-4)

Guidance literature:

With sodium hydride; In dimethyl sulfoxide; at 55 ℃; for 3h;

Reference yield:

7-Azaindole (271-63-6) → C28H31N5O2 (1001014-11-4)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium phosphate / copper(l) iodide; trans-1,2-Diaminocyclohexane / 1,4-dioxane / 19 h / 120 °C

2: sodium hydride / dimethyl sulfoxide / 3 h / 55 °C

With potassium phosphate; sodium hydride; copper(l) iodide; trans-1,2-Diaminocyclohexane; In 1,4-dioxane; dimethyl sulfoxide;

Reference yield:

methyl-[2-(4-nitro-phenyl)-ethyl]-carbamic acid tert-butyl ester (282541-70-2) → C28H31N5O2 (1001014-11-4)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / methanol / 18 h / 2327.23 Torr

2: sodium hydride / dimethyl sulfoxide / 3 h / 55 °C

With hydrogen; sodium hydride; palladium 10% on activated carbon; In methanol; dimethyl sulfoxide;

upstream raw materials:

[2-(4-amino-phenyl)-ethyl]-methyl-carbamic acid tert-butyl ester

4-(1H-pyrrolo[2,3-b]pyridin-1-yl)benzonitrile

7-Azaindole

methyl-[2-(4-nitro-phenyl)-ethyl]-carbamic acid tert-butyl ester

Refernces